A kind of high thermal conductivity ceramic matrix composite material and preparation method thereof
A technology of high thermal conductivity ceramics and composite materials, applied in the field of composite materials, can solve the problem of graphene being difficult to disperse, and achieve the effects of excellent anti-oxidation performance, easy industrial implementation, and simple process
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0043] A preparation method of high thermal conductivity graphene / carbon fiber toughened silicon carbide-zirconium carbide ceramic matrix composite material, the specific steps are:
[0044] 1) The needle-punched carbon fiber reinforcement was treated at a high temperature of 1800 °C for 2 hours, and then deposited in a vapor deposition furnace for 100 hours, 120 hours, and 80 hours, respectively, so that the density of the fiber reinforcement reached 1.02 g / cm 3 ;
[0045] 2) Use a zirconium-silicon integrated resin solution containing graphene oxide to vacuum impregnate the above reinforcement at a pressure of 100Pa for 1 hour, then impregnate at a pressure of 3MPa for 3 hours, and finally pressurize to 10MPa and heat up to 100°C Keep warm for 2 hours at low temperature, 2 hours at 200°C, and 2 hours at 300°C, so that the zirconium-silicon integrated resin is fully cross-linked and cured;
[0046] 3) Place the cured carbon fiber reinforcement in a pyrolysis furnace, and pyr...
Embodiment 2
[0054] A preparation method of high thermal conductivity graphene / carbon fiber toughened silicon carbide-zirconium carbide ceramic matrix composite material, the specific steps are:
[0055] 1) The stitched carbon fiber reinforcement was treated at a high temperature of 1800 °C for 2 hours, and then deposited in a vapor deposition furnace for 100 hours, 100 hours, and 80 hours, respectively, so that the density of the fiber reinforcement reached 1.15 g / cm 3 ;
[0056] 2) Use a zirconium-silicon integrated resin solution containing graphene oxide to vacuum impregnate the above reinforcement at a pressure of 100Pa for 1 hour, then impregnate at a pressure of 3MPa for 3 hours, and finally pressurize to 10MPa and heat up to 100°C Keep warm for 2 hours at low temperature, 2 hours at 200°C, and 2 hours at 300°C, so that the zirconium-silicon integrated resin is fully cross-linked and cured;
[0057] 3) Place the cured carbon fiber reinforcement in a pyrolysis furnace, and pyrolyze ...
Embodiment 3
[0065] A preparation method of high thermal conductivity graphene / carbon fiber toughened silicon carbide-zirconium carbide ceramic matrix composite material, the specific steps are:
[0066] 1) The finely woven and punctured carbon fiber reinforcement was treated at a high temperature of 1800 °C for 2 hours, and then deposited in a vapor deposition furnace for 80 hours, 100 hours, and 80 hours respectively, so that the density of the fiber reinforcement reached 1.16 g / cm 3 ;
[0067] 2) Use a zirconium-silicon integrated resin solution containing graphene oxide to vacuum impregnate the above reinforcement at a pressure of 100Pa for 1 hour, then impregnate at a pressure of 3MPa for 3 hours, and finally pressurize to 10MPa and heat up to 100°C Keep warm for 2 hours at low temperature, 2 hours at 200°C, and 2 hours at 300°C, so that the zirconium-silicon integrated resin is fully cross-linked and cured;
[0068] 3) Place the cured carbon fiber reinforcement in a pyrolysis furnac...
PUM
| Property | Measurement | Unit |
|---|---|---|
| particle diameter | aaaaa | aaaaa |
| density | aaaaa | aaaaa |
| density | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
Login to View More