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Pyrolysis treatment method for oily sludge

A treatment method and sludge technology, applied in pyrolysis treatment of sludge, combustion methods, lighting and heating equipment, etc., can solve the problems of long treatment period, high energy consumption, limited applicability, etc., and achieve low residual oil content, The effect of short treatment cycle and emission compliance

Active Publication Date: 2019-07-26
马平
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0011] The purpose of the present invention is to provide a pyrolysis treatment method for oily sludge, which has the advantages of short treatment period, low energy consumption, up to standard waste gas and waste residue discharge, wide applicability, low residual oil content, etc., and can treat oily sludge thoroughly, Effective, in order to solve the problems of long treatment period, high energy consumption, limited applicability, waste gas and waste residues that cannot meet the emission standards, and high oil content in remaining sludge in the existing technology.

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Examples

Experimental program
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Effect test

Embodiment 1

[0068] Example 1: The waste sulfonated oily sludge produced by drilling in an oilfield in Xinjiang was used as the treatment object, and its moisture content was 25%, oil content was 4%, and silt content was 71%. First, the particle size of the oily sludge is crushed to less than 2 cm, and then enters the pyrolysis device for pyrolysis treatment. The first temperature range is controlled to be 300°C to 450°C, and the time for high-temperature heat treatment of the oily sludge to be treated is 40 minutes. ; The second temperature range is controlled at 450°C to 500°C, and the time for incineration of the oily sludge after the reaction is 20 minutes; the temperature of gas mixed combustion is controlled at 1150°C, and the burning time is 2.5 seconds. The oil content of the waste residue after pyrolysis is 1.035‰, the oily gas produced by pyrolysis is burned at high temperature, and the content of dioxin in the high temperature airflow after combustion is less than 0.1TEQng / Nm 3 ...

Embodiment 2

[0069] Embodiment 2: Taking oil-bearing cuttings produced by drilling in an oil field in Northeast China as the processing object, the water content is 35%, the oil content is 1%, and the rock-bearing rock is 64%. First, the particle size of the oily sludge is crushed to less than 2cm, and then enters the pyrolysis device for pyrolysis treatment. The first temperature range is controlled to be 450°C to 500°C, and the time for high-temperature heat treatment of the oily sludge to be treated is 50 minutes; The second temperature range is controlled from 500°C to 750°C, and the time for incineration of the oily sludge after the reaction is 40 minutes; the temperature of gas mixed combustion is controlled at 1150°C, and the burning time is 2.5 seconds. The oil content of the waste residue after pyrolysis is 1.927‰, the oily gas produced by pyrolysis is burned at high temperature, and the content of dioxin in the high temperature airflow after combustion is less than 0.1TEQng / Nm 3 ...

Embodiment 3

[0070] Example 3: The oily sludge polluted by a chemical plant is used as the treatment object, in which the benzene content is 624 mg / kg, the trichlorethylene content is 2349 mg / kg, the tetrachlorethylene content is 1532 mg / kg and the xylene content is 32 mg / kg. First, the particle size of the oily sludge is crushed to less than 2cm, and then enters the pyrolysis device for pyrolysis treatment. The first temperature range is controlled to be 310°C to 500°C, and the time for high-temperature heat treatment of the oily sludge to be treated is 80 minutes; The second temperature range is controlled from 500°C to 650°C, and the oily sludge after the reaction is incinerated for 30 minutes; the temperature of gas mixed combustion is controlled at 1150°C, and the burning time is 2.5 seconds. The content of benzene in the waste residue after pyrolysis is 0.68 mg / kg, that of trichlorethylene is 1.25 mg / kg, that of tetrachlorethylene is 1.34 mg / kg, and that of xylene is 0.43 mg / kg. The ...

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Abstract

The invention discloses a pyrolysis treatment method for oily sludge. The pyrolysis treatment method for the oily sludge comprises the steps of sequentially carrying out high-temperature heating and incineration treatment on the oily sludge; recovering oil-containing gas generated by high-temperature heating of oil-containing sludge to be treated in a high-temperature heating treatment stage; burning the reacted oily sludge, enabling mixed hot gas generated by burning to flow to a high-temperature heating treatment position to provide heat, enabling the oil content of waste residues generatedby burning to be lower than 3 %o, and enabling the waste residues to be directly buried. Meanwhile, the oil-containing gas, the mixed hot gas and the air are mixed and combusted, and high-temperatureair flows generated by burning flow back respectively to provide heat for high-temperature heating treatment and burning treatment so as to reduce energy consumption and realize energy recycling; andthe remaining high-temperature air flow is purified and discharged. Thus, the pyrolysis treatment method for the oily sludge provided by the invention has the advantages of short treatment period, lowenergy consumption, up-to-standard discharge of waste residues and waste gas and low residual oil content, and is applicable to various types of oily sludge with various oil contents.

Description

technical field [0001] The invention relates to the technical field of process treatment of oily sludge, and more specifically relates to a pyrolysis treatment method of oily sludge. Background technique [0002] Oily sludge refers to the mixture of oil and sediment produced during oil and gas exploration, exploitation, gathering and transportation, and wastewater (liquid) treatment, as well as oily cuttings produced by using oil-based mud during drilling. my country classifies oily sludge as hazardous solid waste, and clearly stipulates that it must be treated in a harmless manner. [0003] At present, the treatment methods of oily sludge include biological treatment, high temperature treatment, incineration, hot washing, solvent extraction, mechanical separation and other methods. However, biological treatment is more suitable for soils polluted by non-dissolved and non-volatile petroleum hydrocarbons, and the hydrocarbon content generally does not exceed 5%. [0004] Th...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C02F11/10F23G5/027F23G7/14
CPCC02F11/10F23G5/027F23G7/14F23G2209/12Y02W10/40
Inventor 吴叶强马平冉宪伟
Owner 马平