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An efficient ni/ni(oh) 2 Hydrogen evolution electrode and preparation method thereof

A hydrogen evolution electrode and electrode technology, applied in the field of hydrogen production, can solve the problems of undiscovered patent documents, etc., and achieve the effects of preventing shedding, improving stability and stable use

Active Publication Date: 2022-02-01
天津市大陆制氢设备有限公司
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0006] Through the search of published patent documents, no published patent documents identical to this patent application have been found

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  • An efficient ni/ni(oh)  <sub>2</sub> Hydrogen evolution electrode and preparation method thereof
  • An efficient ni/ni(oh)  <sub>2</sub> Hydrogen evolution electrode and preparation method thereof
  • An efficient ni/ni(oh)  <sub>2</sub> Hydrogen evolution electrode and preparation method thereof

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Embodiment Construction

[0024] Embodiments of the present invention are described in further detail below in conjunction with the accompanying drawings:

[0025] A high-efficiency Ni / Ni(OH) 2 The innovation of the hydrogen evolution electrode is that the electrode uses nickel sulfate hexahydrate and nickel chloride as the source of nickel elements, and the nickel and its hydroxide nanoparticles are evenly doped by the direct current electrodeposition method combined with the subsequent redox treatment In the catalytic layer, a highly efficient Ni / Ni(OH) 2 Hydrogen evolution electrode.

[0026] The catalytic layer is hemispherical by stacking nano sheet structures, the thickness of the nano sheets is 10-20 nm, and the diameter of the hemisphere is 2-4 μm.

[0027] A high-efficiency Ni / Ni(OH) 2 The hydrogen evolution electrode preparation method is innovative in that it includes the following steps:

[0028] (1) Pretreatment of conductive substrate

[0029] Select the cut nickel foam with a size o...

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Abstract

The invention relates to a high-efficiency Ni / Ni(OH) 2 The hydrogen evolution electrode is characterized in that: the electrode uses nickel sulfate hexahydrate and nickel chloride as the source of nickel elements, and the nickel and its hydroxide nanoparticles are uniformly doped in the catalytic In the layer, a highly efficient Ni / Ni(OH) 2 Hydrogen evolution electrode. The present invention also relates to a method for preparing a high-efficiency Ni / Ni(OH)2 hydrogen evolution electrode, which is characterized in that it includes the following steps: (1) pretreatment of the conductive substrate; (2) preparing nano-sheet nickel and its hydrogen by DC electrodeposition A catalyst layer formed by stacking oxides; (3) performing anodic oxidation treatment to obtain a Ni / Ni(OH)2 hydrogen evolution electrode. The design of the invention is scientific and reasonable, and has the advantages of high catalytic hydrogen evolution activity, low cost, low energy consumption, stable use, good conductivity, etc., and is a highly innovative and efficient Ni / Ni(OH)2 hydrogen evolution electrode and its preparation method .

Description

technical field [0001] The invention belongs to the field of hydrogen preparation, and relates to an electrode, in particular to a high-efficiency Ni / Ni(OH) 2 Hydrogen evolution electrode and its preparation method. Background technique [0002] Modern human life is inseparable from energy. Energy is the foundation of modern economic development and an important strategic material for social development. With the consumption of traditional fossil fuels and the aggravation of environmental pollution, we urgently need to develop a new renewable energy source. At present, the main energy sources for research include hydropower resources, nuclear energy, wind energy, biomass energy, solar energy, hydrogen energy, shale gas, ocean energy, etc. Among the many new energy sources, hydrogen energy is one of the most potential energy sources. [0003] At present, the main source of hydrogen energy is the production of hydrogen from natural gas, coal, or chemical by-products. More t...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C25B11/091C25B1/04C25B11/03C25D3/12C25D9/08C25D11/34
CPCC25B1/04C25D3/12C25D9/08C25D11/34B01J23/755C25B11/057C25B11/031C25B11/051C25B11/075B01J35/33Y02E60/36
Inventor 许卫许莉曹亮亮
Owner 天津市大陆制氢设备有限公司
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