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Medium-temperature daily double-sided crack glaze ceramic and preparation method

A cracked glaze and daily-use technology, which is applied in the field of medium-temperature daily-use double-sided cracked glaze ceramics and preparation, can solve the problems of reducing the breakage rate of finished porcelain, easy volatility, low flexural strength, etc. , the effect of enhancing mechanical strength

Active Publication Date: 2019-09-20
HUNAN HUALIAN CHINA IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] The crackle glaze products currently used in daily tableware ceramics produced by my country are mainly: 1. High silicon and low aluminum (SiO2) 2 63-71%, Al 2 o 3 18-24%) is mainly porcelain, while the crystal phase of high-silicon and low-alumina porcelain is mainly glass phase, and the crystal phase of acicular mullite is less, so its flexural strength is low ( 60MPa or below), so that the damage rate of fried porcelain is high when the product is out of the kiln or after a period of storage after it is out of the kiln; 2. Because of the high damage rate of the product, it is generally used for decoration The surface) is made of cracked glaze, and the outer surface is produced with various non-cracked matte glaze decoration methods to reduce the breakage rate of porcelain; 3. The expansion coefficient of the green body is generally 6.5 to 7.3×10 -6 / °C range, in order to make the glazed surface of the product produce cracks, the matching glaze is generally used with an expansion coefficient of 10-11×10 -6 / °C or above high-expansion glaze, and these high-expansion glazes contain high content of volatile fluxes such as potassium and sodium, which makes the glaze volatile during high-temperature firing and shortens the service life of the kiln

Method used

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  • Medium-temperature daily double-sided crack glaze ceramic and preparation method
  • Medium-temperature daily double-sided crack glaze ceramic and preparation method
  • Medium-temperature daily double-sided crack glaze ceramic and preparation method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] Components and content in the formula of the present invention are:

[0026]

[0027] The mixed mineralizer is a compound of talc and vanadate, and the ratio of talc to vanadate in the mixed mineralizer is 50:1-1.5.

[0028] Accurately formulate the weight of each raw material in the above formula, make mud strips according to the mud making method above, shape the green body, apply glaze, put it in a kiln at 1280°C for 6.5 hours and fire (the firing method is to heat to 1280°C and keep the temperature at 20-25 Minutes, when the temperature drops to 1100°C, keep the temperature for another 30 minutes, and then cool to room temperature naturally), the water absorption test and thermal stability test of the obtained high-alumina daily-use double-sided crack glaze ceramic product are as follows:

[0029] Water absorption test:

[0030]

[0031] Thermal Stability Test:

[0032] Sample serial number Thermal stability (160℃--20℃) A pass B pass ...

Embodiment 2

[0036] Components and content in the formula of the present invention are:

[0037]

[0038] The mixed mineralizer is a compound of talc and vanadate. The ratio of talc to vanadate in the mixed mineralizer is 50:1~1.5.

[0039] Accurately formulate the weight of each raw material in the above formula, make mud sticks according to the mud making method above, shape the green body, apply glaze, put it in a kiln at 1270°C for 6.5 hours and fire (the firing method is to heat to 1270°C and keep the temperature at 20-25 Minutes, when the temperature drops to 1100°C, keep the temperature for another 30 minutes, and then cool to room temperature naturally), the water absorption test and thermal stability test of the obtained high-alumina daily-use double-sided crack glaze ceramic product are as follows:

[0040] Water absorption test:

[0041]

[0042] Thermal Stability Test:

[0043] Sample serial number Thermal stability (160℃--20℃) A pass B pass ...

Embodiment 3

[0047] Components and content in the formula of the present invention are:

[0048]

[0049] The mixed mineralizer is a compound of talc and vanadate. The ratio of talc to vanadate in the mixed mineralizer is 50:1~1.5.

[0050]Accurately formulate the weight of each raw material in the above formula, make mud strips according to the mud making method above, shape the green body, apply glaze, put it in a kiln at 1260°C for 7 hours and fire (the firing method is to heat to 1260°C and keep the temperature at 20-25 Minutes, when the temperature drops to 1100°C, keep the temperature for another 30 minutes, and then cool to room temperature naturally), the water absorption test and thermal stability test of the obtained high-alumina daily-use double-sided crack glaze ceramic product are as follows:

[0051] Water absorption test:

[0052]

[0053] Thermal Stability Test:

[0054] Sample serial number Thermal stability (160℃--20℃) A pass B pass C ...

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Abstract

The invention relates to a medium-temperature daily double-sided crack glaze ceramic and a preparation method. The medium-temperature daily double-sided crack glaze ceramic comprises a preform body and glaze, the preform body is prepared from the following chemical ingredients in mass percent: 57-59% of SiO2, 30-35% of Al2O3, 0.1-0.5% of CaO, 2-2.5% of MgO, 3-3.5% of K2O and 0.1-0.5% of Na2O, and the breaking strength is 100-120MPa; the preparation method of the medium-temperature daily double-sided crack glaze ceramic comprises the following steps: enabling the preform body to be manufactured into a green body, glazing, drying, then carrying out firing treatment, wherein the firing temperature is 1,260-1,280 DEG C, preserving heat for 20-25min, cooling naturally, then preserving the heat for 30min when the temperature drops to 1,100 DEG C, and then cooling continuously to obtain the medium-temperature daily double-sided crack glaze ceramic. The medium-temperature daily double-sided crack glaze ceramic increases the breaking strength of the green body, improves the breaking tenacity of products, and solves the defect that the products are easy to break.

Description

technical field [0001] The invention belongs to the technical field of daily-use ceramics, and in particular relates to a medium-temperature daily-use double-sided cracked glazed ceramic and a preparation method. Background technique [0002] The crackle glaze products currently used in daily tableware ceramics produced by my country are mainly: 1. High silicon and low aluminum (SiO2) 2 63-71%, Al 2 o 3 18-24%) is mainly porcelain, while the crystal phase of high-silicon and low-alumina porcelain is mainly glass phase, and the crystal phase of acicular mullite is less, so its flexural strength is low ( 60MPa or below), so that the damage rate of fried porcelain is high when the product is out of the kiln or after a period of storage after it is out of the kiln; 2. Because of the high damage rate of the product, it is generally used for decoration The surface) is made of cracked glaze, and the outer surface is produced with various non-cracked matte glaze decoration metho...

Claims

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Application Information

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IPC IPC(8): C04B35/185C04B35/622C04B41/86
CPCC04B35/185C04B35/622C04B41/009C04B41/5022C04B41/86C04B2235/3472C04B2235/349C04B2235/656C04B2235/6567C04B2235/96C04B2235/9607
Inventor 麦潮棠钟放平汪大谷柯志勇
Owner HUNAN HUALIAN CHINA IND
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