Spectral selective reflection liquid crystal film and preparation method thereof
A technology of liquid crystal thin film and spectrum selection, applied in liquid crystal materials, chemical instruments and methods, coatings, etc.
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Embodiment 1
[0028] The preparation method of the spectrum selective reflection liquid crystal film is as follows:
[0029] S1. Prepare mixed paint: 4.0% chiral liquid crystal molecules A, 10% nematic liquid crystal molecules B, 15% nematic liquid crystal molecules C, 31% nematic liquid crystal molecules D, 40% nematic liquid crystal molecules E According to the proportion, it is added to the polyurethane-modified acrylic resin with 3 times the quality of cholesteric liquid crystal and 6 times the quality of cholesteric liquid crystal, and in the mixed solution composed of butanone:isophorone=6:4 mixed solvent, fully Stir until the liquid crystal molecules are completely dissolved, and the whole system becomes light yellow with a certain viscosity, then sealed and stored until a film is formed;
[0030] S2. Coating: Apply the thermosetting coating prepared in S1 evenly on the ordinary PET film with a 30 μm wire rod,
[0031] S3. Thermal curing: After coating, place it in an environment of...
Embodiment 2
[0033] The preparation method of the spectrum selective reflection liquid crystal film is as follows:
[0034] S1. Prepare mixed paint: 4.3% chiral liquid crystal molecules A, 15% nematic liquid crystal molecules B, 12.7% nematic liquid crystal molecules C, 38% nematic liquid crystal molecules D, 30% nematic liquid crystal molecules E According to the proportion, it is added to the polyurethane-modified acrylic resin with 4 times the quality of cholesteric liquid crystal and 8 times the quality of cholesteric liquid crystal, and in the mixed solution composed of ethyl acetate:isophorone=5:5 mixed solvent, fully Stir until the liquid crystal molecules are completely dissolved, and the whole system becomes light yellow with a certain viscosity, then sealed and stored until a film is formed;
[0035] S2. Coating: Apply the thermosetting coating prepared in S1 evenly on the ordinary PET film with a 50 μm wire rod;
[0036] S3. Thermal curing: After coating, put it in an environme...
Embodiment 3
[0038] The preparation method of the spectrum selective reflection liquid crystal film is as follows:
[0039] S1. Prepare mixed paint: 4.6% chiral liquid crystal molecules A, 15% nematic liquid crystal molecules B, 12.4% nematic liquid crystal molecules C, 35% nematic liquid crystal molecules D, 33% nematic liquid crystal molecules E Add 4 times the mass of cholesteric liquid crystal polyurethane-modified acrylic resin and 8 times the mass of cholesteric liquid crystal in proportion, and consist of dimethyl carbonate: butyl acetate: isophorone = 4:2:4 mixed solvent In the mixed solution formed, fully stir until the liquid crystal molecules are completely dissolved, and the whole system becomes light yellow with a certain viscosity, and then sealed and stored until a film is formed;
[0040] S2. Coating: apply the thermosetting coating prepared in S1 evenly on the PET film with polyurethane primer with a 20 μm wire rod;
[0041] S3. Thermal curing: after coating, put it in an...
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