A kind of PET blown film bag and preparation method thereof
A film bag and biphenyl technology, applied in the field of PET blown film bags and their preparation, can solve the problems of inability to use transparent film bags, easy delamination, etc., achieve high economic value and social value, improve mechanical properties, resistance Excellent flammability and mechanical properties
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Embodiment 1
[0030] A PET blown film bag is characterized in that it is made of the following raw materials in parts by weight: 60 parts of PET resin, silane-based ionized modified poly 3,3-difluoro-[1,1-biphenyl]- 30 parts of 4,4-dicarboxylic acid N,N-dihydroxyethylaniline ester, 2 parts of nano boron fiber, 3 parts of sepiolite powder, 1 part of (triethoxysilyl) acetic acid, tris(2,4- Di-tert-butyl) phenyl phosphite 0.3 part, salicylate ultraviolet absorber 0.1 part, paraffin 0.2 part.
[0031] The preparation method of the silane-based ionized modified poly-3,3-difluoro-[1,1-biphenyl]-4,4-dicarboxylate N,N-dihydroxyethylaniline comprises the following steps:
[0032]Step S1: Add 1.54kg of 3,3-difluoro-[1,1-biphenyl]-4,4-dicarboxylic acid, 1kg of N,N-dihydroxyethylaniline, and 0.3kg of tetrabutyl titanate to In 9kg of dimethyl sulfoxide, stir for 25 minutes to obtain a reaction solution, then transfer the reaction solution to a high-pressure reactor, replace the air in the reactor with ...
Embodiment 2
[0038] A PET blown film bag is characterized in that it is made of the following raw materials in parts by weight: 65 parts of PET resin, silane-based ionized modified poly 3,3-difluoro-[1,1-biphenyl]- 33 parts of 4,4-dicarboxylic acid N,N-dihydroxyethylaniline, 3 parts of nano-boron fiber, 4 parts of sepiolite powder, 1.5 parts of (triethoxysilyl) acetic acid, tris(2,4 - 0.35 parts of di-tert-butylphenyl) ester, 0.15 parts of benzophenone-based ultraviolet absorber, and 0.25 parts of polydimethylsiloxane.
[0039] The preparation method of the silane-based ionized modified poly-3,3-difluoro-[1,1-biphenyl]-4,4-dicarboxylate N,N-dihydroxyethylaniline comprises the following steps:
[0040] Step S1: Add 1.54kg of 3,3-difluoro-[1,1-biphenyl]-4,4-dicarboxylic acid, 1kg of N,N-dihydroxyethylaniline ester, and 0.4kg of titanium dioxide to N,N - in 11 kg of dimethylformamide, stirred for 27 minutes to obtain a reaction solution, and then transferred the reaction solution to a high-p...
Embodiment 3
[0046] A PET blown film bag is characterized in that it is made of the following raw materials in parts by weight: 70 parts of PET resin, silane-based ionized modified poly 3,3-difluoro-[1,1-biphenyl]- 35 parts of 4,4-dicarboxylic acid N,N-dihydroxyethylaniline ester, 3.5 parts of nano boron fiber, 5.5 parts of sepiolite powder, 2 parts of (triethoxysilyl) acetic acid, bis(2,4- 0.4 part of di-tert-butylphenyl) pentaerythritol diphosphite, 0.2 part of benzotriazole ultraviolet absorber, and 0.3 part of paraffin.
[0047] The preparation method of the silane-based ionized modified poly-3,3-difluoro-[1,1-biphenyl]-4,4-dicarboxylate N,N-dihydroxyethylaniline comprises the following steps:
[0048] Step S1: Add 1.54kg of 3,3-difluoro-[1,1-biphenyl]-4,4-dicarboxylic acid, 1kg of N,N-dihydroxyethylaniline, and 0.45kg of titanium chloride to N, In 13 kg of N-dimethylacetamide, stir for 30 minutes to obtain a reaction solution, then transfer the reaction solution to a high-pressure re...
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