Braille printing ink and preparation method of Braille printed matter
A technology for printing ink and Braille, applied in the directions of reproduction/marking method, printing, ink, etc., can solve the problems of poor adhesion, easy falling off of bump characters, high cost of Braille printing equipment and materials, and achieves good antibacterial effect and is not easy to fall off. , the effect of strong adhesion
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[0024] In the present invention, various existing methods for extracting organic compounds can be used for the extraction of the terpenoids. According to a preferred embodiment of the present invention, the extraction method of the terpenoids comprises:
[0025] (1) ultrasonically treating the alcohol solution of the natural plant powder, and filtering the ultrasonic product to obtain the extract of the natural plant;
[0026] (2) Adding an extractant to the extract for extraction to obtain an extract containing the terpenoids.
[0027] In the present invention, the natural plant powder can be ground into powder by conventional methods. Preferably, the particle size of the natural plant powder can be 1-1000 μm.
[0028] In the present invention, ultrasonic devices in the prior art can be used to ultrasonically treat the alcohol solution of the natural plant powder, as long as the active ingredients in the natural plant powder can be fully dissolved in the alcohol solution. A...
preparation example 1
[0060] Used to illustrate the extraction method of terpenoids one
[0061] (1) Grind lavender into powder, take 100g of powdered lavender, add it to 800mL of ethanol solution, soak it for 24h and stir evenly, slowly add the above-mentioned lavender-ethanol mixture in an ultrasonic circulation device, and the dropping rate is 100mL / min , After the dropwise addition, ultrasonication was intense for 1h, and the ultrasonic power was 3000W. The mixed solution was filtered, and the filtrate was poured into a 1L flask for distillation. After distillation, the liquid in the flask was lavender solution.
[0062] (2) Take 20 g of lavender liquid and add sodium silicate solution to adjust the pH value to 12. After fully stirring, add ethyl acetate to extract four times. The ethyl acetate extract is distilled under reduced pressure at 110° C. to obtain primary terpenoids. Primary terpenoids are separated and purified through a silica gel chromatographic column, and the eluent is chlorofor...
preparation example 2
[0064] Used to illustrate the extraction method of terpenoids II
[0065] (1) Lemongrass is ground into powder, get 100g powdery lemongrass, join in the ethanol solution of 600mL, stir after soaking 24h, slowly add above-mentioned lemongrass ethanol mixture dropwise in the ultrasonic circulation device, the rate of addition is 100mL / min, strong ultrasonication for 1h after the dropwise addition, ultrasonic power 3000W, filter the mixed solution, pour the filtrate into a 1L flask, and carry out distillation. The liquid in the flask after distillation is citronella grassland liquid.
[0066] (2) Take 20 g of citronella prairie liquid and add sodium hydroxide solution to adjust the pH value to 14. After stirring well, add petroleum ether to extract four times. The petroleum ether extract is subjected to vacuum distillation at 100° C. to obtain primary terpenoids. The primary terpenoids are separated and purified through a silica gel chromatographic column, and the eluent is chlor...
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