Preparation method of high-solid-content PAE resin paper wet strength agent
A technology of high solid content and wet strength agent, applied in paper, reinforcing agent addition, papermaking, etc., can solve the problems of high transportation cost of PAE resin, low solid content of PAE resin, reduce transportation cost, etc., and achieve excellent storage stability, Excellent wet reinforcement effect and reduced transportation cost
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specific Embodiment example 1
[0019] Add 81 g of diethylenetriamine and 0.5 g of 98% sulfuric acid to a 1 L three-necked flask equipped with a stirrer, a thermometer, a reflux condenser, and a nitrogen inlet tube, feed nitrogen, slowly add 111 g of adipic acid, and control the temperature at Below 130°C, if the temperature exceeds 130°C, cooling and cooling treatment is required; after adding adipic acid, start to heat up, when the temperature reaches 170°C, keep warm for 4 hours, after the warming reaction is over, start cooling, when the temperature drops to 80°C, add 130g of deionized water, continue to cool down to 30°C, when the temperature is stable, add 90.3g of epichlorohydrin dropwise to the reaction kettle, the dropping time is controlled at 40 minutes, and the dropwise addition of mixed monomers is controlled Temperature to 40°C and keep warm for 6 hours, start cooling, when the temperature drops to 25°C, add 16g of 98% sulfuric acid and 350g of deionized water to the reaction kettle, adjust the ...
specific Embodiment example 2
[0021] Add 101 g of diethylenetriamine and 0.8 g of 98% sulfuric acid to a 1 L three-necked flask equipped with a stirrer, a thermometer, a reflux condenser, and a nitrogen inlet tube, feed nitrogen, slowly add 111 g of adipic acid, and control the temperature at Below 130°C, if the temperature exceeds 130°C, cooling and cooling treatment is required; after adding adipic acid, start to heat up, when the temperature reaches 170°C, keep warm for 4 hours, after the warming reaction is over, start cooling, when the temperature drops to 80°C, add 147g of deionized water, continue to cool down to 30°C, when the temperature is stable, add 70g of epichlorohydrin dropwise to the reaction kettle, the dropping time is controlled at 40 minutes, and the temperature is controlled after the addition of the mixed monomer is completed To 40 ℃ and keep warm for 6 hours, the reaction is over, start cooling, when the temperature drops to 25 ℃, add 21g of 98% sulfuric acid and 360g of deionized wat...
specific Embodiment example 3
[0023] Add 81 g of diethylenetriamine and 0.5 g of 98% sulfuric acid to a 1 L three-necked flask equipped with a stirrer, a thermometer, a reflux condenser, and a nitrogen inlet tube, feed nitrogen, slowly add 111 g of adipic acid, and control the temperature at Below 130°C, if the temperature exceeds 130°C, cooling and cooling treatment is required; after the addition of adipic acid, start to heat up, when the temperature reaches 170°C, keep warm for 4 hours, after the keep warm, start cooling, when the temperature drops to 80°C, add 130g of deionized water, continue to cool down to 30°C, when the temperature is stable, add 70g of epichlorohydrin dropwise to the reaction kettle, the dropping time is controlled at 40 minutes, and the temperature is controlled after the addition of the mixed monomer is completed To 40 ℃ and keep warm for 6 hours, the reaction is over, start cooling, when the temperature drops to 25 ℃, add 21g of 98% sulfuric acid and 300g of deionized water to t...
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