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Additive with angelica sinensis fragrance style characteristics, preparation method thereof and cigarette containing additive

A technology of additives and aroma, applied in the field of tobacco, can solve the problems of unguaranteed product quality stability, hidden dangers of product quality stability, unreported research, etc., and achieves the effects of good application prospects, rich aroma and simple composition.

Active Publication Date: 2020-09-29
CHINA TOBACCO YUNNAN IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] The natural angelica fragrance spices on the market are mainly angelica extracts. There are differences in raw material varieties caused by different factors such as soil, climate, and growth environment, and the stability of product quality cannot be guaranteed; at the same time, because its preparation process is mainly through organic solvent leaching , Steam distillation and other separation and enrichment methods, the obtained products are more or less mixed with ineffective ingredients such as pigments and vegetable waxes that affect the quality of the aroma; it has laid a hidden danger for the stability of product quality in the food and daily chemical industry
[0003] At present, the existing technology is mainly aimed at the research on the extraction process of angelica extract or spices, and there is no report on the research on the characteristic additive of angelica fragrance style through compounding of components

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0036] Take 50 mg of 3-propylidene-1-isobenzofuranone by mass; 4 mg of isovaleric acid; 0.5 mg of ethyl caprate and 1 kg of glycerol triacetate and mix them at room temperature for 30 minutes to make the raw materials fully Dissolve, prepare a homogeneous solution, put it in barrels, store it in a dark and cool place, and store it for 48 hours to obtain additive D.

[0037] The additive D was added to the cigarette filter in an amount of 1 μL / filter tip, and the cigarette sample was rolled with Yunyan (Ruanzhen) leaf group, and the other auxiliary materials and additives were kept unchanged, and the cigarette sample 4 was prepared, which was the same as Yunyan (Ruanzhen) products were compared and evaluated, and it was found that the richness of aroma increased by 5%, the irritation decreased by 3%, the miscellaneous gas decreased by 2.5%, and the fragrance of angelica increased by 9%.

Embodiment 2

[0039] Mix 10 mg of 3-propylidene-1-isobenzofuranone; 0.2 mg of isovaleric acid; 0.1 mg of ethyl caprate and 1 kg of 60% ethanol, shake at room temperature for 10 minutes to fully dissolve the raw materials, Prepare a homogeneous solution, fill it into barrels, store it in a dark and cool place, and store it for 12 hours to obtain Additive E.

[0040] The additive E was sprayed onto the surface of the cigarette paper at a rate of 0.5mL / 100g of paper, and the cigarette sample was rolled with Hongtashan (classic) leaves, and the remaining auxiliary materials and additives were kept unchanged, and the cigarette sample 5 was prepared. Compared with Hongtashan (classic) products, it was found that the richness of aroma increased by 2%, the irritation decreased by 2%, the aroma of angelica increased by 4%, the miscellaneous gas decreased by 2%, and the comfort of smoke increased by 0.4%.

Embodiment 3

[0042] 20 mg of 3-propanediene-1-isobenzofuranone; 2 mg of isovaleric acid; 0.2 mg of ethyl caprate and 1 kg of 1:1 propylene glycol / glycerol were mixed, and shaken at room temperature for 20 min to make The raw materials are fully dissolved, prepared into a homogeneous solution, filled into barrels, placed in a dark and cool place, and stored for 24 hours to obtain additive F.

[0043] The additive F was sprayed onto the surface of shredded tobacco in an amount of 1.00mL / 100g shredded tobacco, and a cigarette sample was rolled with Hongtashan (Legend) leaves, and the remaining auxiliary materials and additives were kept unchanged. (Legend) products were compared and evaluated, and found that: the richness of aroma increased by 4%, the irritation decreased by 5%, the miscellaneous gas decreased by 4%, and the aroma of angelica increased by 5%.

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Abstract

The invention discloses an additive with angelica sinensis aroma style characteristics. Based on the weight of the additive with the angelica sinensis aroma style characteristics, the additive comprises the 10 to 50mg / kg of 3-propylene-1-isobenzofuranone; 0.2 to 4 mg / kg of isovaleric acid; and 0.1 to 0.5 mg / kg of ethyl caprate. According to the preparation method, the 3-propylene-1-isobenzofuranone with medicinal herb flavor, the isovaleric acid with sour taste, the ethyl caprate with fruit wine flavor and a solvent are combined to prepare the additive with the angelica sinensis flavor style characteristics, and the additive has obvious angelica sinensis flavor and rich fragrance. The additive with the angelica sinensis aroma style characteristic is added into the cigarette, the cigarettearoma amount can be increased, the cigarette is endowed with the obvious angelica sinensis aroma, and the effects of increasing the cigarette aroma richness, reducing stimulation, relieving offensiveodor, increasing the angelica sinensis aroma and improving the cigarette smoking comfort are achieved.

Description

technical field [0001] The invention belongs to the technical field of tobacco, and in particular relates to an additive with the style characteristics of angelica fragrance and a cigarette containing the additive. Background technique [0002] The natural angelica fragrance spices on the market are mainly angelica extracts. There are differences in raw material varieties caused by different factors such as soil, climate, and growth environment, and the stability of product quality cannot be guaranteed; at the same time, because its preparation process is mainly through organic solvent leaching , steam distillation and other separation and enrichment methods, the obtained products are more or less mixed with ineffective ingredients such as pigments and vegetable waxes that affect the quality of aroma; this has laid a hidden danger for the stability of product quality in the food and daily chemical industries. [0003] At present, the prior art is mainly aimed at the research...

Claims

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Application Information

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IPC IPC(8): A24D3/14A24D1/02A24B15/30
CPCA24D3/14A24D1/02A24B15/305
Inventor 张凤梅刘志华蔡炳彪司晓喜蒋薇朱瑞芝吴丽君向能军唐石云李振杰何沛王昆淼刘春波杨晨苏钟璧
Owner CHINA TOBACCO YUNNAN IND
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