Preparation method of electrode plate for copper-silver ion generating device
An ion generating device and electrode plate technology, applied in chemical instruments and methods, water/sludge/sewage treatment, water/sewage treatment, etc., can solve the problems of low efficiency and high cost, achieve uniform fusion, complete alloying, Precise controllable effect of alloy ratio
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Embodiment 1
[0027] Embodiment 1: This embodiment provides a method for preparing an electrode plate for a copper-silver ion generating device, which includes the following steps:
[0028] (1) Preparation of raw materials: the electrolytic copper and silver ingots are immersed in a mixed solution of 20% sulfuric acid and 5% hydrofluoric acid for 20 to 40 minutes, and then washed with pure water for use;
[0029] (2) Melting: The electrolytic copper and silver ingots are placed in a crucible according to weight percentages: 70% to 99% of electrolytic copper and 1% to 30% of silver ingots, and the crucible is placed in a double vacuum smelting device equipped with a constant electromagnetic field In the vacuum degree of 10 -3 , Rotate the crucible under the condition of 1000℃~1200℃ to form electromagnetic two-way stirring, and keep the temperature for 100min~150min, and cool down with ionized water for no more than 30min to obtain copper-silver alloy;
[0030] (3) Cold working: cold forging, cold r...
Embodiment 2
[0044] Embodiment 2: This embodiment provides a method for preparing an electrode plate for a copper-silver ion generating device. The steps are basically the same as those of Embodiment 1, except that it includes the following steps:
[0045] (1) Preparation of raw materials: the electrolytic copper and silver ingots are soaked in a mixed solution of 20% sulfuric acid and 5% hydrofluoric acid for 20 minutes, and then washed with pure water for use;
[0046] (2) Melting: The electrolytic copper and silver ingots are placed in a crucible according to weight percentages: 91% of electrolytic copper and 9% of silver ingots, and the crucible is placed in a double vacuum smelting equipment with a constant electromagnetic field. The vacuum is 10 -3 , Under the condition of 1000℃, rotate the crucible to form electromagnetic two-way stirring, and keep it for 100min, use ionized water to cool down the temperature, the cooling time is not more than 30min, to obtain the copper-silver alloy;
[0...
Embodiment 3
[0061] Embodiment 3: This embodiment provides a method for preparing an electrode plate for a copper-silver ion generating device. The steps are basically the same as those in Embodiments 1 and 2, except that it includes the following steps:
[0062] (1) Preparation of raw materials: the electrolytic copper and silver ingots are immersed in a mixed solution of 20% sulfuric acid and 5% hydrofluoric acid for 40 minutes, and then washed with pure water for use;
[0063] (2) Melting: The electrolytic copper and silver ingots are placed in a crucible according to weight percentages: 99% of electrolytic copper and 1% of silver ingots, and the crucible is placed in a double vacuum melting device with a constant electromagnetic field. 10 -3 , Under the condition of 1200℃, rotate the crucible to form electromagnetic two-way stirring, and keep it for 150min, use ionized water to cool down the temperature, the cooling time is not more than 30min, to obtain the copper-silver alloy;
[0064] (3) ...
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