Fumigation liquid for lung-yin deficiency type xerophthalmia and preparation thereof
A technology of lung yin deficiency and fumigation liquid, which is applied to medical preparations containing active ingredients, drug delivery, plant raw materials, etc., can solve the problems of pill diameter loss, high packaging cost, unpleasant smell, etc. Presence, prevent oxidation and escape, ensure pure natural effect
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Embodiment 1
[0039] Prescription: 12 parts of raw land, 10 parts of Ophiopogon japonicus, 15 parts of Scrophulariaceae, 9 parts of white peony, 9 parts of paeonol, 6 parts of mulberry leaves and 16 parts of chrysanthemum.
[0040] Take the above-mentioned medicinal materials, crush them to 20-40 meshes respectively, then weigh them according to the above-mentioned amount, and mix them evenly in the extraction kettle. Carbon dioxide was used as the medium for supercritical fluid extraction for 3 hours, and the first extract was obtained from the separation tank.
[0041] Then adjust the pressure of the extraction kettle to 35MPa, the temperature to 45°C, the pressure to the separation kettle to 6MPa, and the temperature to 20°C, and use 20% ethanol as the medium to carry out supercritical fluid extraction for 2 hours to obtain the extract I; Kettle pressure 6MPa, temperature 30°C, use 60% ethanol as the medium to carry out supercritical fluid extraction for 3 hours to obtain extract II; the...
Embodiment 2
[0044] Prescription: 12 parts of raw land, 10 parts of Ophiopogon japonicus, 15 parts of Scrophulariaceae, 9 parts of white peony, 9 parts of paeonol, 6 parts of mulberry leaves and 16 parts of chrysanthemum.
[0045] Take the above-mentioned medicinal materials, crush them to 20-40 meshes respectively, then weigh them according to the above-mentioned amount, and mix them evenly in the extraction kettle. Carbon dioxide was used as the medium for supercritical fluid extraction for 3 hours, and the first extract was obtained from the separation tank.
[0046] Then adjust the pressure of the extraction kettle to 35MPa, the temperature to 45°C, the pressure to the separation kettle to 6MPa, and the temperature to 20°C, and perform supercritical fluid extraction with 20% ethanol as the medium for 3 hours to obtain the second extract with an extraction rate of 78.0%.
[0047] The first extract and the second extract are mixed evenly to obtain a fumigant that can treat dry eye syndro...
Embodiment 3
[0049] Prescription: 12 parts of raw land, 10 parts of Ophiopogon japonicus, 15 parts of Scrophulariaceae, 9 parts of white peony, 9 parts of paeonol, 6 parts of mulberry leaves and 16 parts of chrysanthemum.
[0050]Take the above-mentioned medicinal materials, crush them to 20-40 meshes respectively, then weigh them according to the above-mentioned amount, and mix them evenly in the extraction kettle. Carbon dioxide was used as the medium for supercritical fluid extraction for 3 hours, and the first extract was obtained from the separation tank.
[0051] Adjust the pressure of the extraction kettle to 30MPa, the temperature to 40°C, the pressure to the separation kettle to 6MPa, and the temperature to 30°C, and conduct supercritical fluid extraction with 60% ethanol as the medium for 3 hours to obtain the second extract with an extraction rate of 87.1%.
[0052] The first extract and the second extract are mixed evenly to obtain a fumigant that can treat dry eye syndrome of ...
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