Solid electrolyte membrane and all-solid-state battery comprising same
A technology of solid electrolyte membrane and solid electrolyte, which is applied in the direction of solid electrolyte, non-aqueous electrolyte battery, electrolyte, etc., can solve the problems of battery short circuit and short circuit, and achieve the effect of preventing electric short circuit and inhibiting the growth of lithium dendrites
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Embodiment 1
[0111] (1) Preparation of the first solid electrolyte layer
[0112] Polyethylene oxide (PEO, Mw=4,000,000 g / mol) was dissolved in acetonitrile (AN) as a solvent to prepare a 4% by weight polymer solution. At this point, LiTFSI was introduced together as a lithium salt such that [EO] / [Li + ] The mol ratio=18 / 1. The polymer solution was stirred overnight at 70 °C to fully dissolve the PEO and lithium salt therein. Next, an additive solution including an initiator and a curing agent is prepared. Curing agent is PEGDA (Mw=575), initiator is benzoyl peroxide (BPO), wherein, based on PEO, the consumption of polyethylene glycol diacrylate (PEGDA) is 20% by weight, and based on PEGDA, the amount of BPO The dosage is 1%. Acetonitrile was used as solvent. The additive solution was stirred for about 1 hour so that the introduced ingredients could be thoroughly mixed. Then, the additive solution is added to the polymer solution, and the two solutions are thoroughly mixed with each ...
Embodiment 2
[0120] A solid electrolyte membrane was obtained in the same manner as in Example 1, except that HAuCl with a concentration of 5% by weight was used in the preparation of the solid electrolyte layer 4 ·3H 2 O.
Embodiment 3
[0122] A solid electrolyte membrane comprising the first solid electrolyte layer, the suppression layer, the second solid electrolyte layer, the suppression layer and the third solid electrolyte layer stacked in sequence is obtained. The solid electrolyte membrane of Example 3 has a structure different from that of the solid electrolyte membrane of Example 1 to which an additional suppression layer and a third solid electrolyte layer are added. Each layer was prepared in the same manner as in Example 1.
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Abstract
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