A kind of cemented carbide that strengthens Co-Ni base binding phase by Si and preparation method thereof
A cemented carbide and binder phase technology, applied in the field of cemented carbide, can solve the problems of easy agglomeration and limited strengthening effect, and achieve the effect of improving the bending strength at room temperature and high temperature, realizing industrialization, and simple and controllable process.
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Embodiment 1
[0022] Pre-wet grinding 0.6wt% of the total weight of silicon carbide powder with a particle size of 0.6 μm for 6 hours, then adding 10wt% cobalt powder, 10wt% nickel powder and the remainder of tungsten carbide powder and then wet grinding for 18 hours, After the wet grinding mixture is spray-dried and pressed into shape; after the compact is sintered in a low-pressure liquid phase at 1450 ° C, a pressure of 0.6 MPa, and a holding time of 1 h, the Si-enhanced Co-Ni binder phase of the present invention can be obtained. quality alloy.
[0023] Characterize the microstructure of the cemented carbide prepared in this embodiment, its structure is as follows figure 1 As shown, the ordered phase is the strengthening phase, and the phase structure is A3B (where A represents Co and / Ni elements, and B represents Si elements).
Embodiment 2~9
[0033] The preparation process of Examples 2-9 is basically the same as that of Examples, and its specific proportioning and process parameters are as shown in Table 1.
[0034] Table 1 The preparation parameters of the cemented carbide regeneration process of Example 1-Example 9 and some comparative examples
[0035]
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