Iron-chromium-aluminum alloy with pink oxide film and its preparation method and annealing furnace
An iron-chromium-aluminum alloy, oxide film technology, applied in anodizing, furnaces, manufacturing tools, etc., can solve the problems of uneven color, bending and poor torsional performance, and achieve high annealing temperature, good performance and long service life. Effect
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[0038] As an implementation of the embodiment of the present invention, the diameter of the drawn iron-chromium-aluminum alloy wire is 4-12 mm.
[0039] S2, placing the clean iron-chromium-aluminum alloy wire into a nitrate solution for passivation to obtain an iron-chromium-aluminum alloy wire with a passivation film;
[0040] This process has two functions: firstly, it has the function of neutralizing the residual alkali solution; secondly, it has the function of passivation, and its electrolyte has oxidizing properties, which can not only oxidize the metal ions and the replaced hydrogen atoms, but even the atomic state. Oxygen can oxidize on the surface of the alloy, and the chemical potential of atomic oxygen is high. At the same time as the oxidation of the electrolyte, atomic oxygen will chemically adsorb on the surface of the alloy. In chemical adsorption, O has electron-withdrawing properties and Metals have the property of losing electrons, so O can extract electrons ...
Embodiment 1
[0062] Embodiment 1 provides a kind of preparation method of the iron-chromium-aluminum alloy with pink oxide film, as follows:
[0063] 1. Put the drawn iron-chromium-aluminum alloy wire with a diameter of 10mm into the lye solution at a temperature of 95 ℃, keep it warm for 1.5h, clean the lubricant on the surface of the iron-chromium-aluminum alloy wire, and the solute in the lye solution and the solute. The mass concentrations are shown in Table 1.
[0064] 2. Put the iron-chromium-aluminum alloy wire after cleaning the lubricant in step 1 into boiling water at 100°C for ultrasonic cleaning for 10 minutes.
[0065] 3. Put the iron-chromium-aluminum alloy wire cleaned in step 2 into a sodium nitrate solution with a mass fraction of 55% sodium nitrate and a temperature of 15°C for electrolytic passivation for 25s, then take it out and put it into boiling water at 100°C for ultrasonic cleaning for 10 minutes.
[0066] 4. Put the iron-chromium-aluminum alloy wire treated in s...
Embodiment 2
[0071] Embodiment 2 provides a kind of preparation method of the iron-chromium-aluminum alloy with pink oxide film, is specifically as follows:
[0072] 1. Put the drawn iron-chromium-aluminum alloy wire with a diameter of 8mm into the lye solution at a temperature of 100 ℃, keep it warm for 1.8h, clean the lubricant on the surface of the iron-chromium-aluminum alloy wire, and the solute in the lye solution and the solute. The mass concentrations are shown in Table 1.
[0073] 2. Put the iron-chromium-aluminum alloy wire after cleaning the lubricant in step 1 into boiling water at 100°C for ultrasonic cleaning for 10 minutes.
[0074] 3. Put the iron-chromium-aluminum alloy wire cleaned in step 2 into a sodium nitrate solution with a mass fraction of 60% sodium nitrate and a sodium nitrate solution with a temperature of 35°C for 30s, then take it out and put it into boiling water at 100°C for ultrasonic cleaning for 10 minutes.
[0075] 4. Put the iron-chromium-aluminum alloy...
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