A system for purifying antibiotics in drinking water from a waterworks
A technology for purifying water plants and drinking water, applied in multi-stage water/sewage treatment, light water/sewage treatment, adsorption water/sewage treatment, etc., can solve problems such as the increase of drug-resistant bacteria, infection, and difficulty in removing antibiotics from drinking water , to achieve the effect of simple and strong response of the degradation device
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Embodiment 1
[0031] 1. Preparation of Degradable Gel Bands
[0032] (1) The Bi (NO 3 ) 3 ·5H 2O 18g, Zn(NO 3 ) 2 ·6H 2 O 10g, FeCl 3 7g, NaNO 3 A mixed solution prepared with 1g, HMT 16g, AcOH 2g, and deionized water 250mL, boiled at 105°C, refluxed for 40h, cooled to room temperature, filtered, washed, vacuum freeze-dried at -80°C for 20h, and ground through a 200-mesh sieve to obtain FeZnBi- NO 3 -LDHs powder;
[0033] (2) Under the protection of Ar, FeZnBi-NO 3 - 40 g of LDHs powder was added to 500 mL of formamide, stirred at a speed of 1000 rpm for 7 days, centrifuged at 2500 rpm, and the filtrate was collected to obtain a stripped LDHs colloidal solution;
[0034] (3)N 2 Under the protection, 10 g of N-methyl maleic acid monoamide monomer was weighed and dissolved in 40 mL of deionized water, then 50 g of methyl 2-(hydroxymethyl) acrylate, 300 g of distilled water were added successively, and the solution was fully sonicated for 30 min. Mix evenly, and place it in a bro...
Embodiment 2
[0044] 1. Preparation of Degradable Gel Bands
[0045] (1) The Bi (NO 3 ) 3 ·5H 2 O 19g, Zn(NO 3 ) 2 ·6H 2 O 11g, FeCl 3 7.5g, NaNO 3 A mixed solution prepared with 1.1g, 17g HMT, 2.5g AcOH, and 250-300mL deionized water, boiled at 108°C, refluxed for 44h, cooled to room temperature, filtered, washed, vacuum freeze-dried at -70°C for 22h, ground through a 200-mesh sieve, get FeZnBi-NO 3 -LDHs powder;
[0046] (2) Under the protection of Ar, FeZnBi-NO 3 - 45 g of LDHs powder was added to 550 mL of formamide, stirred at a speed of 1150 rpm for 8 days, centrifuged at 2750 rpm, and the filtrate was collected to obtain a stripped LDHs colloidal solution;
[0047] (3)N 2 Under the protection, 11 g of N-methyl maleic acid monoamide monomer was weighed and dissolved in 45 mL of deionized water, then 55 g of methyl 2-(hydroxymethyl) acrylate and 350 g of distilled water were added successively, and the solution was fully sonicated for 35 min. Mix evenly, and place it in a...
Embodiment 3
[0057] 1. Preparation of Degradable Gel Bands
[0058] (1) The Bi (NO 3 ) 3 ·5H 2 O 20g, Zn(NO 3 ) 2 ·6H 2 O 12g, FeCl 3 8g, NaNO 3 A mixed solution prepared with 1.2g, 18g HMT, 3g AcOH, and 250-300mL deionized water, boiled at 110°C, refluxed for 48h, cooled to room temperature, filtered, washed, vacuum freeze-dried at -60°C for 24h, ground through a 200-mesh sieve, get FeZnBi-NO 3 -LDHs powder;
[0059] (2) Under the protection of Ar, FeZnBi-NO 3 - 50 g of LDHs powder was added to 600 mL of formamide, stirred at a speed of 1300 rpm for 9 days, centrifuged at 3000 rpm, and the filtrate was collected to obtain a stripped LDHs colloidal solution;
[0060] (3)N 2 Under the protection, 12 g of N-methyl maleic acid monoamide monomer was weighed and dissolved in 50 mL of deionized water, and then 60 g of methyl 2-(hydroxymethyl) acrylate, 400 g of distilled water were added successively, and the solution was fully sonicated for 40 min. Mix evenly, and place it in a br...
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