Adhesive composition for optical irradiation peeling, laminate body, and laminate body production method and peeling method
An adhesive and light irradiation technology, applied in bonding methods, chemical instruments and methods, semiconductor/solid-state device manufacturing, etc., can solve problems such as large wafer damage, and achieve the effects of excellent dispersibility and good light absorption capacity
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[0169] (1) Mixer: Rotation and revolution mixer ARE-500 made by THINKY Co., Ltd.
[0170] (2) Viscosity measurement: Toki Sangyo Co., Ltd. rotational viscometer TVE-22H
[0171] (3) Measurement of transmittance: UV2550 ultraviolet-visible spectrophotometer manufactured by Shimadzu Corporation
[0172] (4) Vacuum bonding device: SUSS MicroTec Co., Ltd., manual bonding machine (Manual Bonder)
[0173] (5) 308nm laser irradiation device: manufactured by SUSS MicroTec Co., Ltd., 308nm laser irradiation device
[0174] (6) Infrared radiation thermometer: manufactured by TESTO Co., Ltd., infrared radiation thermometer 835-H1
[0175] (7) 532nm laser irradiation device: LT-2137 manufactured by Lotus-TII
[0176] [1] Preparation of composition
preparation example 1
[0178] 95 g of vinyl-containing MQ resin (manufactured by Wacker Chemie) as polysiloxane (a1), 93.4 g of p-menthane (manufactured by Nippon Terpene Chemical Co., Ltd.) as a solvent, and 0.41 g of 1,1-diphenyl-2-propyn-1-ol (manufactured by Tokyo Chemical Industry Co., Ltd.) of the polymerization inhibitor (A3) was stirred with a stirrer for 5 minutes.
[0179] To the obtained mixture was added Si—H group-containing linear polydimethylsiloxane (manufactured by Wacker Chemie) having a viscosity of 100 mPa·s as polysiloxane (a2), polysiloxane (a2) (a1) 29.5 g of vinyl-group-containing linear polydimethylsiloxane (manufactured by Wacker Chemie) having a viscosity of 200 mPa·s, and viscosity of polydimethylsiloxane as component (B) 1,000,000 mm 2 / s polyorganosiloxane (manufactured by Wacker Chemie, trade name AK1000000), and 0.41 g of 1-ethynyl-1-cyclohexanol (manufactured by Wacker Chemie) as (A3), were stirred for 5 minutes with a stirrer.
[0180] 14.9 g of the following mixtu...
preparation example 2
[0183] 95 g of vinyl-containing MQ resin (manufactured by Wacker Chemie) as polysiloxane (a1), 93.4 g of p-menthane (manufactured by Nippon Terpene Chemical Co., Ltd.) as a solvent, and 0.41 g of 1,1-diphenyl-2-propyn-1-ol (manufactured by Tokyo Chemical Industry Co., Ltd.) of the polymerization inhibitor (A3) was stirred with a stirrer for 5 minutes.
[0184] To the obtained mixture was added Si—H group-containing linear polydimethylsiloxane (manufactured by Wacker Chemie) having a viscosity of 100 mPa·s as polysiloxane (a2), polysiloxane (a2) (a1) 23.6 g of vinyl-group-containing linear polydimethylsiloxane (manufactured by Wacker Chemie) having a viscosity of 200 mPa·s, and viscosity of polydimethylsiloxane as component (B) 1,000,000 mm 2 / s polyorganosiloxane (manufactured by Wacker Chemie, trade name AK1000000), and 0.41 g of 1-ethynyl-1-cyclohexanol (manufactured by Wacker Chemie) as (A3), were stirred for 5 minutes with a stirrer.
[0185] To the obtained mixture was a...
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