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Anti-corrosion treatment method for sintered NdFeB permanent magnet

A processing method and technology of permanent magnets, which are applied in the manufacture of permanent magnets, inductors/transformers/magnets, solid-state diffusion coatings, etc., to achieve the effects of easy popularization and application, simple operation process, and good corrosion resistance.

Active Publication Date: 2022-04-15
TIANJIN SANHUAN LUCKY NEW MATERIAL CO LTD +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, there is no relevant report on the way of treating NdFeB permanent magnet materials by zinc shedding

Method used

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  • Anti-corrosion treatment method for sintered NdFeB permanent magnet

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] Grind 3.5kg of ¢24*¢15*18mm NdFeB permanent magnet material in a vibration mill for 2 hours. After degreasing and degreasing with sodium phosphate 20g / liter, sodium carbonate 10g / liter and sodium hydroxide 10g / liter, use 60-mesh white corundum, sandblasting and derusting, and then surface cleaning (ultrasonic washing method) and antirust drying to obtain the surface For permanent magnet materials with roughness RA=0.6μm, 96 parts of zinc powder (weight ratio) and 4 parts of rare earth powder dysprosium are processed by high-energy ball milling, and D50 is 0.15 microns. After mixing evenly, put it together with the magnet, raise the temperature to 380°C, keep it for 15 minutes, take it out, remove the light in a vibration mill, and passivate it. The properties of the anti-corrosion NdFeB permanent magnet material are shown in Table 1.

Embodiment 2

[0026] Polish 3.5 kg of ¢24*¢15*18mm NdFeB permanent magnet material according to the method of Example 1 for 2 hours, use 60 mesh corundum, derust with nitric acid, and then clean the surface (ultrasonic water washing method) and dry for antirust 5微米。 To obtain a permanent magnet material with a surface roughness RA=0.35μm, zinc powder (weight ratio) 99 parts, rare earth powder terbium 1 part, through high-energy ball milling, wherein D50 is 0.5 microns. After mixing evenly, put it together with the magnet, raise the temperature to 350°C, keep it for 60 minutes, take it out, remove the light in a vibration mill, and passivate it. The properties of the anti-corrosion NdFeB permanent magnet material are shown in Table 1.

Embodiment 3

[0028] Polish 3.5 kg of ¢24*¢15*18mm NdFeB permanent magnet material according to the method of Example 1, sand blast and derust, use 80 mesh brown corundum, and then clean the surface (ultrasonic water washing method) and rust-proof and dry To obtain a permanent magnet material with a surface roughness RA=0.4 μm, 98 parts of zinc powder (weight ratio), 1 part of rare earth powder dysprosium, and 1 part of metal terbium are processed by high-energy ball milling, wherein D50 is 3 microns. After mixing evenly, put it together with the magnet, raise the temperature to 380°C, keep it for 45 minutes, take it out, remove the light in a vibration mill, and passivate it. The properties of the anti-corrosion NdFeB permanent magnet material are shown in Table 1.

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Abstract

The present invention provides an anti-corrosion treatment method for sintered NdFeB permanent magnets. The anti-corrosion treatment method adopts powder thermal galvanizing, and includes the following steps: substrate pretreatment → galvanizing → galvanizing post-treatment, wherein, The zincizing agent added in the zincizing step does not contain any chloride ions. The zincizing agent includes a mixture of zinc powder and rare earth powder. Due to the adoption of the above technical scheme, the sintered NdFeB permanent magnet treated by the anticorrosion treatment method of the present invention has a uniform and dense zinc layer, good anticorrosion performance, no loss to the magnet, and can be used continuously.

Description

technical field [0001] The invention belongs to the technical field of anticorrosion treatment of NdFeB permanent magnets, and in particular relates to an anticorrosion treatment method of sintered NdFeB permanent magnets. Background technique [0002] In recent years, the application and development of NdFeB permanent magnet materials has been very rapid, and the success of the protection of NdFeB permanent magnet materials is one of the key technologies related to the promotion and application of materials. The material is mainly made of rare earth metals such as neodymium Nd, iron and boron through powder metallurgy process. As the strongest magnetic material at present, it has been widely used in electroplating devices, machinery, medical treatment, automobiles and other fields, and its application prospects are very broad. [0003] The premise of the application of NdFeB permanent magnet materials is to first solve the anti-corrosion problem of NdFeB permanent magnet m...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C23C10/36H01F41/02
CPCC23C10/36H01F41/026
Inventor 白晓刚于海华潘广麾仉新功聂源航韩雪胡蝶
Owner TIANJIN SANHUAN LUCKY NEW MATERIAL CO LTD