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Cement grinding aid and preparation method thereof

A cement grinding aid, a technology of the cement industry, applied in the field of cement manufacturing, can solve the problems of wide distribution of cement particles and reduce the strength of cement, achieve uniform and stable fineness and specific surface area, reduce grinding energy consumption, fineness and The effect of specific surface area retention

Pending Publication Date: 2022-01-28
SICHUAN SEDAR CHEM
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The purpose of the present invention is to provide a cement grinding aid and its preparation method, to solve the technical problem that the liquid grinding aid in the prior art tends to have a wide distribution range of cement particles and reduce the strength of cement

Method used

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  • Cement grinding aid and preparation method thereof

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] Preparation of cement grinding aids:

[0030] 1.1. Raw materials

[0031] Its preparation includes the following raw materials in parts by weight: 80 parts of cement industrial wastewater; 5 parts of high-alumina fly ash; 3 parts of ethylene glycol; 25 parts of triethanolamine; 8 parts of molasses; 3 parts of sodium acetate; 18 parts of sodium dialkylbenzene sulfonate; 6 parts of polyoxyethylene alkylamine.

[0032] 1.2, preparation method, comprises the following steps:

[0033] S1, filter and remove impurities from the cement industry wastewater;

[0034] S2. Add triethanolamine into the reaction vessel, add filtered cement industrial wastewater under stirring, and obtain mixture A after stirring at a stirring rate of 2000 rpm and a temperature of 45° C. for 20 minutes;

[0035] S3. In the state of stirring, sequentially add sodium acetate and sodium sulfate to the mixture A, and after stirring at a stirring rate of 2000 rpm and a temperature of 80°C for 40 minutes...

Embodiment 2

[0039] Preparation of cement grinding aids:

[0040] 2.1. Raw materials

[0041] Its preparation includes the following raw materials in parts by weight: 60 parts of cement industrial wastewater; 2 parts of high aluminum fly ash; 9 parts of ethylene glycol; 15 parts of triethanolamine; 5 parts of molasses; 6 parts of sodium acetate; 8 parts of sodium dialkylbenzene sulfonate; 12 parts of polyoxyethylene alkylamine.

[0042] 2.2, preparation method, comprises the following steps:

[0043] S1, filter and remove impurities from the cement industry wastewater;

[0044] S2. Add triethanolamine into the reaction vessel, add filtered cement industrial wastewater under stirring, and stir at a stirring rate of 900 rpm and a temperature of 35° C. for 30 minutes to obtain a mixture A;

[0045] S3. In the state of stirring, add sodium acetate and sodium sulfate in sequence to mixture A, and obtain mixture B after stirring at a stirring rate of 900 rpm and a temperature of 65° C. for 60...

Embodiment 3

[0049] Preparation of cement grinding aids:

[0050] 3.1. Raw materials

[0051] Its preparation includes the following raw materials in parts by weight: 75 parts of cement industrial wastewater; 3 parts of high-alumina fly ash; 7 parts of ethylene glycol; 18 parts of triethanolamine; 7 parts of molasses; 4 parts of sodium acetate; 10 parts of sodium dialkylbenzene sulfonate; 9 parts of polyoxyethylene alkylamine.

[0052] 3.2, preparation method, comprise the following steps:

[0053] S1, filter and remove impurities from the cement industry wastewater;

[0054] S2. Add triethanolamine into the reaction vessel, add filtered cement industrial wastewater under stirring, and obtain mixture A after stirring at a stirring rate of 1200 rpm and a temperature of 40° C. for 25 minutes;

[0055] S3. In the state of stirring, add sodium acetate and sodium sulfate in sequence to the mixture A, and after stirring at a stirring rate of 1200 rpm and a temperature of 70° C. for 55 minutes...

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Abstract

The invention discloses a cement grinding aid and a preparation method thereof, and solves the technical problems that a liquid grinding aid in the prior art is easy to cause wide cement particle distribution range and low cement strength. The cement grinding aid is prepared from the following raw materials in parts by weight: 60-80 parts of cement industrial wastewater, 2-5 parts of high-alumina fly ash, 3-9 parts of ethylene glycol, 15-25 parts of triethanolamine, 5-8 parts of molasses, 3-6 parts of sodium acetate, 8-10 parts of sodium sulfate, 8-18 parts of an anionic surfactant, and 6-12 parts of a nonionic surfactant. According to the cement grinding aid and the preparation method thereof, the production cost is low, the fineness of cement particles is reduced, the specific surface area of the cement particles is increased, and the strength of cement can be improved.

Description

technical field [0001] The invention relates to the technical field of cement production, in particular to a cement grinding aid and a preparation method thereof. Background technique [0002] In the grinding process of cement clinker, adding a small amount of additional substances (liquid or solid substances), which can significantly improve the grinding efficiency or reduce energy consumption without damaging the performance of cement, is generally called cement grinding aid. agent. Cement grinding aid is a chemical additive that improves the grinding effect and performance of cement. It can significantly increase the output of cement table, the strength of cement of all ages, and improve its fluidity. Cement grinding aids can greatly reduce the phenomenon of electrostatic adsorption and ball formation during the grinding process, and can reduce the tendency of re-agglomeration of ultrafine particles formed during the grinding process. Cement grinding aids can also signi...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B24/32C04B103/52
CPCC04B40/0039C04B2103/52C04B22/0006C04B18/08C04B24/026C04B24/10C04B24/04C04B22/147C04B24/20C04B24/32
Inventor 余建华张秋萍王正凯杨凯董振鹏于学龙
Owner SICHUAN SEDAR CHEM