Two-pack type adhesive, multilayer body, molded body and packaging material
A technology of adhesives and packaging materials, applied in packaging, wrapping paper, adhesives, etc., can solve the problems of poor heat sealing and insufficient oxygen barrier properties, and achieve excellent formability
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[0188] Hereinafter, specific synthesis examples and examples are given to describe the present invention in detail, but the present invention is not limited to these examples. In addition, in the following examples, "parts" and "%" represent "parts by mass" and "% by mass", respectively, unless otherwise specified.
[0189]
Synthetic example 1
[0190] (Synthesis Example 1) Synthesis of Polyester Polyol (A1-1)
[0191] Using 300.3 parts of isophthalic acid, 300.3 parts of terephthalic acid, 37.7 parts of neopentyl glycol, 101.0 parts of ethylene glycol, and 260.7 parts of 1,9-nonanediol, a polyester polyol was synthesized according to a conventional method. The obtained polyester polyol was diluted with ethyl acetate to a resin solid content of 60%, and the number average molecular weight (Mn) was 3000, the weight average molecular weight (Mw) was 16,000, and the resin hydroxyl value (solid content conversion) was 19.2 mgKOH / g. Polyester polyol (A1-1) having a resin acid value (solid content conversion) of 0.55 mgKOH / g and a glass transition temperature (Tg) of 10.7°C.
Synthetic example 2
[0192] (Synthesis Example 2) Synthesis of Polyester Polyol (A1-2)
[0193] Using 424.8 parts of isophthalic acid, 182.0 parts of terephthalic acid, 57.1 parts of neopentyl glycol, 215.8 parts of 1,6-hexanediol, 34.0 parts of ethylene glycol, and 3-methyl-1,5-pentanediol 86.3 parts, synthetic polyester polyol according to conventional method. The obtained polyester polyol was diluted with ethyl acetate to a resin solid content of 60% to obtain a number average molecular weight (Mn) of 11,200, a weight average molecular weight (Mw) of 25,900, and a resin hydroxyl value (solid content conversion) of 10.8 mgKOH / g. Polyester polyol (A1-2) having a resin acid value (solid content conversion) of 2.2 mgKOH / g and a glass transition temperature (Tg) of 15.8°C.
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