Application of wilforlide A inhalation preparation in medicine for treating lung inflammation
A technology of triptolide A and inhalation preparations, applied in drug combination, drug delivery, antipyretics, etc., to achieve low bioavailability, high safety, and avoid systemic adverse reactions
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Embodiment 1
[0015] Embodiment 1 contains the preparation of triptolide A (Wilforlide A) powder spray
[0016] References [Que Huiqing, Geng Yingying, Lin Sui, Li Yuanchao. Study on the chemical constituents of Tripterygium wilfordii [J]. Chinese herbal medicine, 2005(11): 1624-1625.] Extracted triptolide A, and micronized it into triptolide after extraction Raw material of rattan lactone A (Wilforlide A, WA).
[0017] Referring to [Feng Li. Development of aztreonam lung inhalation powder aerosol [D]. Chongqing Medical University, 2007.] The method in the article, and according to the characteristics of the drug in this experiment, appropriately modified, weighed triptolide A ( WilforlideA, WA) raw material 2g, glycine 3g, lactose 1g, WA was dissolved in 100mL of absolute ethanol, magnetically stirred for 30min, after WA was completely dissolved, glycine and lactose were dissolved in 30mL of water under magnetic stirring, and slowly added into the ethanol solution of WA, after the solutio...
Embodiment 2
[0020] The influence of embodiment 2 different doses of WA powder aerosol on pulmonary inflammation
[0021] Refer to [Zhang Yaping, Selection of acute pneumonia model in rats induced by lipopolysaccharide inhalation through different routes[J]. Chinese Journal of Experimental Formulas, 2018,24(07):82-88.] part 2.2.1, through nebulization inhalation A method for making an animal model of pneumonia with LPS and making appropriate adjustments. After 3 days of continuous modeling, continue modeling for 4 days, and simultaneously utilize the rat respiratory tract dosing device to give the powder aerosol in embodiment 1 (dose is set to be 0mg / kg, 1mg / kg , 2mg / kg, 4mg / kg, 8mg / kg; dosage is based on active ingredient WA); set non-modeling normal animal group simultaneously as negative control; adopt oral administration of hormone methylprednisolone 10mg / kg as positive control ( hormone group). For the degree of inflammation and index detection methods in each animal group, refer to...
Embodiment 3W
[0032] Embodiment 3WA absorption kinetics in vivo
[0033] Reference [WANG Z, YEUNG S, CHEN S, et al.Bioavailability of wilforlide A inmice and its concentration determination using an HPLC-APCI-MS / MS method[J].JChromatogr B Analyt Technol Biomed Life Sci,2018,1090:65 -72.] The measurement method is to measure the systemic bioavailability of WA through powder spray administration, so as to investigate the degree and risk of systemic distribution of WA after powder spray administration.
[0034] SD rats were divided into groups (4 in each group) and given WA powder aerosol (based on WA content) inhalation administration of 1 mg / kg, 2 mg / kg, 4 mg / kg, 8 mg / kg; intravenous administration of 1 mg / kg. According to the time point of the above reference method, blood was taken, measured, and kinetic parameters were calculated, and the bioavailability of other groups was calculated with AUC0-∞ of intravenous injection as 100%.
[0035] Part of the pharmacokinetic parameters measured a...
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