Inorganic porous membrane
A porous membrane and inorganic technology, applied in the field of inorganic porous membrane and its formation, can solve problems such as twists and turns, irregular pores, and poor microstructure
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[0083] Material
[0084] Commercially available alumina powders were purchased from SUMITOMO CHEMICAL (Japan), including type AA-04 (grain size 0.5 μm, used to prepare the feed composition for the top active layer) and Type AA-3 (grain size 3.4 μm, used to prepare the feed composition for the buffer layer). Surfactant F127 powder was purchased from SIGMA-ALDRICH (Singapore) and used without further purification. Obtain a commercially available porous ceramic substrate support (e.g., polycrystalline Al 2 o 3 ).
[0085] Gradient film preparation method
[0086] An alumina suspension / paste was prepared by adding 27 wt% alumina powder to deionized water. Subsequent 17wt% F127 powder was added to the suspension and allowed to stand in a refrigerator at a temperature of 6° C. for about 20 hours to dissolve. After gentle and thorough stirring at a temperature of 2-8°C, a feed composition is obtained. The feed composition was then dip-coated layer by layer on a porous cera...
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