Slow-digestion resistant dextrin and preparation method thereof
A resistant dextrin, slow technology, applied in the field of preparation of slowly digested resistant dextrin, can solve the problem of uncontrollable glycosidic bond ratio
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[0023] The invention provides a method for preparing slow digestion resistant dextrin, comprising the following steps:
[0024] 1) mixing starch and water to obtain starch milk;
[0025] 2) Mixing the starch milk obtained in the step 1) with α-medium temperature amylase, reacting for 30-45 minutes, then adding pullulanase and maltotriose generating enzyme at the same time, performing synergistic enzymolysis to obtain an enzymolysis solution;
[0026] 3) The enzymatic hydrolyzate obtained in step 2) is sequentially subjected to evaporation, concentration and polymerization to obtain a crude product of slowly digestible resistant dextrin;
[0027] 4) Purifying the crude slow digestion resistant dextrin obtained in step 3) to obtain slow digestion resistant dextrin.
[0028] The invention mixes starch and water to obtain starch milk.
[0029] In the present invention, the starch is preferably corn starch, tapioca starch, wheat starch or pea starch, more preferably corn starch; ...
Embodiment 1
[0052] A preparation method for slowly digesting resistant dextrin, comprising the following steps:
[0053] 1) Mix cornstarch and reverse osmosis water, and adjust the Baume degree of starch milk to 17°Bé;
[0054] 2) First mix the starch milk obtained in step 1) with 1.2×10 8 Mix Uα-medium temperature amylase, after 30 minutes of reaction, add 1.25×10 7 U pullulanase and 5.25 x 10 6 U maltotriose generating enzyme, pH 5.0, 52°C, and then enzymatically hydrolyzed for 120 minutes to obtain an enzymatic hydrolyzate with a maltotriose content of 71%;
[0055] 3) Evaporate and concentrate the enzymolysis solution obtained in step 2) in the reaction kettle, the pressure is -0.075MPa, the temperature is 90°C, and the mass percentage content of the solid is evaporated to 82%; add according to 0.5% of the mass of the obtained concentrated solution Citric acid, keep vacuum -0.09MPa, temperature 140°C, react for 40min.
[0056] 4) Dissolve the slowly digested resistant dextrin crud...
Embodiment 2
[0059] A preparation method for slowly digesting resistant dextrin, comprising the following steps:
[0060] 1) Mix corn starch and reverse osmosis water, and adjust the Baume degree of starch milk to 16°Bé;
[0061] 2) First mix the starch milk obtained in step 1) with 2.4×10 8 Mix Uα-medium temperature amylase, react for 45min, then add 2×10 7 U pullulanase and 4.5 x 10 6 U maltotriose generating enzyme, pH 5.3, 54°C, and then enzymatically hydrolyzed for 180 minutes to obtain an enzymatic hydrolyzate with a maltotriose content of 72%;
[0062] 3) Evaporate and concentrate the enzymolysis solution obtained in step 2) in the reaction kettle, the pressure is -0.06MPa, the temperature is 95°C, and the mass percentage content of the solid is evaporated to 83%; according to 1.25% of the mass of the obtained concentrated solution, add Phosphoric acid, keep vacuum -0.06MPa, temperature 148°C, react for 32min.
[0063] 4) Dissolve the slowly digested resistant dextrin crude prod...
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