Polymer capable of being used for pigment coating, polymer-coated pigment, preparation method of polymer-coated pigment and inorganic coating
A technology for coating pigments and polymers, applied in the field of pigments, can solve the problems of easy flocculation, no color solution, poor long-term stability, etc., and achieve good long-term storage stability, excellent long-term stability, and good alkali resistance. Effect
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[0063] According to a second aspect of the present invention, the above-mentioned preparation method of the polymer that can be used for pigment coating comprises the following steps:
[0064] Mix the diol polymer with isophorone diisocyanate for reaction, and then add polyetheramine for capping reaction to obtain a polymer that can be used for pigment coating;
[0065] Wherein, the diol polymer comprises any one or a combination of at least two of polyethylene glycol polyethers, polypropylene glycol polyethers or polycarbonate diols;
[0066] Polyetheramines include the polyetheramine designated Jeffamine M2070.
[0067] Only by reacting isophorone diisocyanate with the above-mentioned specific types of diol polymers and specific types of polyether amines can the polymers with the above-mentioned specific structures be obtained, and the pigments can be protected while covering the pigments, so that the pigments can be used at high temperatures. It has better persistence in a...
Embodiment approach
[0069] As an optional embodiment of the present invention, the reaction temperature of the diol polymer and isophorone diisocyanate is 60-90°C, and the reaction time is 1-4h.
[0070] Typical but non-limiting reaction temperatures are 60°C, 62°C, 64°C, 65°C, 66°C, 68°C, 70°C, 72°C, 74°C, 75°C, 76°C, 78°C, 79°C, 80°C °C, 81 °C, 82 °C, 84 °C, 85 °C, 86 °C, 88 °C or 90 °C, typical but non-limiting reaction times are 1 h, 2 h, 3 h or 4 h.
[0071] As an optional embodiment of the present invention, the temperature of the capping reaction is 40-50° C., and the reaction time is 2-3 hours.
[0072] A typical but non-limiting capping reaction temperature is 40°C, 42°C, 44°C, 45°C, 46°C, 48°C or 50°C, and a typical but non-limiting reaction time is 2h, 2.5h or 3h.
[0073] According to a third aspect of the present invention, there is also provided a polymer-coated pigment, including an inorganic pigment, a polymer coated on the surface of the inorganic pigment, and optional additives...
Embodiment 1
[0112] This embodiment provides a kind of polymer that can be used for pigment encapsulation, and the preparation method of this polymer comprises the following steps:
[0113] Put 2000 grams of polycarbonate diol PCDL2000 (dihydric alcohol with a number average molecular weight of 2000) into a completely dry glass reactor, raise the temperature to 100±2°C, stir, vacuum dehydrate and degas for 3 hours, and cool down to 40±2°C ℃, then add 444.64 grams of IPDI, react at 80±2℃ for 2 hours, cool down to 40℃, add 4000 grams of Jeffamine M2070 for capping, and react for 2 hours to obtain a polymer that can be used for pigment coating.
[0114] The prepared polymer that can be used for pigment coating has a general structural formula shown in formula (1).
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