Silicon carbide coating graphite base and preparation method thereof
A technology of silicon carbide coating and graphite base, applied in the field of silicon carbide coating graphite base and its preparation, can solve the problems of poor thermal shock resistance and corrosion resistance, uneven particle size of silicon carbide coating and the like , to achieve the effect of improving thermal shock resistance and corrosion resistance, enhancing bonding force and reducing the degree of aggregation
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Embodiment 1
[0040]A specific embodiment of the structure of a silicon carbide coated graphite base of the present invention: it includes a graphite base, the graphite base is in the shape of a disk, and a silicon carbide film is deposited on the surface of the graphite base, and the thickness of the silicon carbide film is 50-200nm; a graphene film is deposited outside the silicon carbide film, and the silicon carbide film is used as a substrate for graphene epitaxial growth, and the thickness of the graphene film is 100-300nm; a silicon carbide coating is deposited on the surface of the graphene film.
[0041] The deposited graphene has a large specific surface area (the specific surface area of graphene is about 2600m 2 / g, about 1000 times that of graphite), which can increase the nucleation sites of chemical vapor deposition silicon carbide. Therefore, when silicon carbide is deposited outside the graphene film, the degree of aggregation of silicon carbide grains on the graphene fil...
Embodiment 2
[0052] The structure specific embodiment two of a kind of silicon carbide coating graphite base of the present invention: comprise graphite base, graphite base is disk plate shape, is deposited with silicon carbide film on the surface of graphite base, the thickness of silicon carbide film is 50-200nm; a refractory metal carbide layer is deposited outside the silicon carbide film, and the silicon carbide film is used as a substrate for the epitaxial growth of refractory metal carbide, and a silicon carbide coating is deposited on the surface of the refractory metal carbide layer; refractory metal The surface energy of carbide is large, which is conducive to the growth of fine silicon grains. In this embodiment, the refractory metal carbide layer is a tantalum carbide layer; in other embodiments, the refractory metal carbide layer may also be a tungsten carbide layer, a titanium carbide layer or a molybdenum carbide layer.
[0053] The method for preparing the silicon carbide c...
Embodiment 3
[0062] The third specific embodiment of the structure of a silicon carbide coated graphite base of the present invention: it includes a graphite base, and the graphite base is in the shape of a disk; the surface of the graphite base is deposited with a refractory metal carbide layer, and the refractory metal A silicon carbide coating is deposited on the surface of the material layer; the surface energy of the refractory metal carbide is large, which is conducive to the growth of fine silicon grains. In this embodiment, the refractory metal carbide layer is a tantalum carbide layer; in other embodiments, the refractory metal carbide layer may also be a tungsten carbide layer, a titanium carbide layer or a molybdenum carbide layer.
[0063] The method for preparing the silicon carbide coated graphite base in this embodiment comprises the following steps:
[0064] Step 1: Pretreat the graphite base and place it in a chemical vapor deposition chamber;
[0065] Step 2: vacuumize t...
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Abstract
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