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Silicon carbide coating graphite base and preparation method thereof

A technology of silicon carbide coating and graphite base, applied in the field of silicon carbide coating graphite base and its preparation, can solve the problems of poor thermal shock resistance and corrosion resistance, uneven particle size of silicon carbide coating and the like , to achieve the effect of improving thermal shock resistance and corrosion resistance, enhancing bonding force and reducing the degree of aggregation

Pending Publication Date: 2022-04-19
GONG YI VAN-RES INNOVATION COMPOSITE MATERIAL CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0005] In view of this, the purpose of the present invention is to provide a silicon carbide coated graphite base, to solve the uneven particle size of the silicon carbide coating in the prior art, poor thermal shock resistance and corrosion resistance in the MOCVD environment ; In addition, the application also provides a method for making a silicon carbide coated graphite base

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  • Silicon carbide coating graphite base and preparation method thereof
  • Silicon carbide coating graphite base and preparation method thereof
  • Silicon carbide coating graphite base and preparation method thereof

Examples

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Embodiment 1

[0040]A specific embodiment of the structure of a silicon carbide coated graphite base of the present invention: it includes a graphite base, the graphite base is in the shape of a disk, and a silicon carbide film is deposited on the surface of the graphite base, and the thickness of the silicon carbide film is 50-200nm; a graphene film is deposited outside the silicon carbide film, and the silicon carbide film is used as a substrate for graphene epitaxial growth, and the thickness of the graphene film is 100-300nm; a silicon carbide coating is deposited on the surface of the graphene film.

[0041] The deposited graphene has a large specific surface area (the specific surface area of ​​graphene is about 2600m 2 / g, about 1000 times that of graphite), which can increase the nucleation sites of chemical vapor deposition silicon carbide. Therefore, when silicon carbide is deposited outside the graphene film, the degree of aggregation of silicon carbide grains on the graphene fil...

Embodiment 2

[0052] The structure specific embodiment two of a kind of silicon carbide coating graphite base of the present invention: comprise graphite base, graphite base is disk plate shape, is deposited with silicon carbide film on the surface of graphite base, the thickness of silicon carbide film is 50-200nm; a refractory metal carbide layer is deposited outside the silicon carbide film, and the silicon carbide film is used as a substrate for the epitaxial growth of refractory metal carbide, and a silicon carbide coating is deposited on the surface of the refractory metal carbide layer; refractory metal The surface energy of carbide is large, which is conducive to the growth of fine silicon grains. In this embodiment, the refractory metal carbide layer is a tantalum carbide layer; in other embodiments, the refractory metal carbide layer may also be a tungsten carbide layer, a titanium carbide layer or a molybdenum carbide layer.

[0053] The method for preparing the silicon carbide c...

Embodiment 3

[0062] The third specific embodiment of the structure of a silicon carbide coated graphite base of the present invention: it includes a graphite base, and the graphite base is in the shape of a disk; the surface of the graphite base is deposited with a refractory metal carbide layer, and the refractory metal A silicon carbide coating is deposited on the surface of the material layer; the surface energy of the refractory metal carbide is large, which is conducive to the growth of fine silicon grains. In this embodiment, the refractory metal carbide layer is a tantalum carbide layer; in other embodiments, the refractory metal carbide layer may also be a tungsten carbide layer, a titanium carbide layer or a molybdenum carbide layer.

[0063] The method for preparing the silicon carbide coated graphite base in this embodiment comprises the following steps:

[0064] Step 1: Pretreat the graphite base and place it in a chemical vapor deposition chamber;

[0065] Step 2: vacuumize t...

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Abstract

The invention relates to a silicon carbide coating graphite base which comprises a disc-shaped graphite base body, a silicon carbide film is deposited on the surface of the graphite base body, and a graphene film or a refractory metal carbide layer is deposited outside the silicon carbide film. Or a refractory metal carbide layer is deposited on the surface of the graphite base; the silicon carbide coating is deposited on the surface of the refractory metal carbide layer or the surface of the graphene film; a graphene film or a refractory metal carbide layer is deposited on the surface of a graphite base, so that the specific surface area of the surface of a matrix is greatly increased, more nucleation sites are formed on the surface of the matrix, and when a silicon carbide coating is deposited, the aggregation degree of silicon carbide crystal grains is reduced, so that the crystal grains of the silicon carbide coating are distributed more uniformly and compactly; the thermal shock resistance and the corrosion resistance of the silicon carbide coating graphite base are improved; the invention further relates to a preparation method of the silicon carbide coating graphite base.

Description

technical field [0001] The invention belongs to the technical field of semiconductor epitaxial growth equipment, and in particular relates to a silicon carbide coated graphite base and a preparation method thereof. Background technique [0002] MOCVD equipment is the most important equipment in the production process of the LED industry. Due to its high technical content, its value accounts for 70% of the entire industrial chain (epitaxial wafer-chip-package-application). The CVD-SiC coated graphite base is the carrier and heating body of the substrate material, and is the most critical component of the MOCVD equipment, which directly determines the uniformity and purity of the thin film material. The bonding force between the silicon carbide coating and the substrate, surface roughness, compactness, purity and other indicators directly affect the quality of the epitaxial wafer and the life of the graphite base. [0003] The preparation method of silicon carbide coated grap...

Claims

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Application Information

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IPC IPC(8): C04B41/87
CPCC04B41/87C04B41/009C04B41/5059C04B35/522C04B41/4531
Inventor 张东生姚栋嘉李江涛王征魏庆渤吴恒
Owner GONG YI VAN-RES INNOVATION COMPOSITE MATERIAL CO LTD
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