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Preparation method of continuous efficient green surfactant

A surfactant and high-efficiency technology, which is applied in the field of preparation of continuous and high-efficiency green surfactants, can solve the problems of reducing the preparation efficiency of alkyl glycosides, the viscosity of alkyl glycosides, and reducing the defoaming efficiency, etc. Continuous use, beneficial to mass production, and the effect of improving production efficiency

Pending Publication Date: 2022-04-26
JIANGSU WAN QI BIOLOGICAL TECH
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Alkyl glycosides generally have a darker color and need to be decolorized and bleached. Due to the high viscosity of high-concentration alkyl glycosides and poor fluidity, a certain stirring speed is required in a general-purpose bleacher. This requires the use of defoaming equipment for auxiliary production
[0004] The most widely used defoaming method today is the thermal defoaming method, but in the existing thermal defoaming method, it is easy to cause serious fouling in the heater, which will greatly reduce its defoaming efficiency and increase energy consumption, thereby affecting Decolorization efficiency, reducing the production efficiency of alkyl glycosides

Method used

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  • Preparation method of continuous efficient green surfactant
  • Preparation method of continuous efficient green surfactant
  • Preparation method of continuous efficient green surfactant

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Embodiment

[0047] see Figure 1-10 , a kind of preparation method of continuous efficient type green surfactant, comprises the steps:

[0048] S1. Alkylation reaction: According to the configuration formula, put the raw materials for the production of alkyl glycosides into the mixing equipment and mix them at a temperature of 95-130°C;

[0049] S2. Dealcoholization treatment: the mixed solution after the alkylation reaction is subjected to multi-stage vacuum dealcoholization treatment at a temperature of 130-160° C. to obtain a pretreated product;

[0050] S3. Stirring decolorization: put the pretreated product and decolorizing agent into the decolorization furnace 1, and use the stirring device 2 to stir the solution to complete the product decolorization requirements;

[0051] S4. Defoaming: During the stirring process, use the heating rod 201 to heat the solution to eliminate the bubbles generated during the decolorization stirring;

[0052] S5. Descaling: During the defoaming proce...

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Abstract

The invention discloses a preparation method of a continuous high-efficiency green surfactant, and belongs to the field of surfactant preparation, the preparation method of the continuous high-efficiency green surfactant comprises the following steps: alkylation reaction: adding alkyl glycoside production raw materials into mixing equipment according to a preparation formula, and mixing and stirring at 95-130 DEG C; carrying out dealcoholization treatment; stirring and decolorizing; defoaming is performed; descaling is conducted; filtering and compounding; in the process of stirring and defoaming by using the heating rod, the intermittent effect of the self-stripping moving ring is increased to assist in stripping dirt in the elastic guide pipe, reduce the energy consumption of the heater and improve the heating and defoaming efficiency, so that the production efficiency of alkyl glycoside is effectively improved. In addition, the dirt treated in time can also prevent loss of alkyl glycoside components in the decoloration process due to too high heat of the heater, and the production quality of the alkyl glycoside is effectively improved through the effect of the self-stripping moving ring.

Description

technical field [0001] The invention relates to the field of surfactant preparation, in particular to a method for preparing a continuous high-efficiency green surfactant. Background technique [0002] Green surfactants refer to surfactants that are processed from natural or renewable resources, are less irritating to the human body and are easily biodegradable. Alkyl glucoside is a new type of green surfactant that emerged in the 1990s. It is a mixture obtained by losing a molecule of the hemiacetal group of glucose and fatty alcohol group in the catalysis of acid, a natural renewable resource. product. Alkyl glycosides have low surface tension, no cloud point, adjustable HLB value, strong wetting power, strong detergency, rich and delicate foam, strong compatibility, non-toxic, harmless, non-irritating to the skin, and rapid and thorough biodegradation. It can be compounded with any type of surfactant and has obvious synergistic effect, so it is widely used as a green su...

Claims

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Application Information

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IPC IPC(8): C07H1/00C07H1/06C07H15/04C07G3/00B01J19/18B01J19/00
CPCC07H1/00C07H1/06C07H15/04C07G3/00B01J19/18B01J19/0013B01J2219/00076Y02P20/10
Inventor 金瑞刘建文
Owner JIANGSU WAN QI BIOLOGICAL TECH