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Method for testing and evaluating self-healing property of graphene microcapsule asphalt

An evaluation method and microcapsule technology, applied in the direction of applying repeated force/pulsation force to test material strength, measuring device, strength characteristics, etc., can solve the problem that the self-healing evaluation method of asphalt is not applicable to the self-healing evaluation of asphalt with graphene microcapsules and other issues to achieve an accurate evaluation

Active Publication Date: 2022-05-13
HARBIN INST OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The purpose of the present invention is to solve the problem that the existing asphalt self-healing evaluation method is not suitable for graphene microcapsule asphalt self-healing evaluation, to provide a graphene microcapsule asphalt self-healing test evaluation method and to propose corresponding evaluation This method provides an effective means for the accurate evaluation of the self-healing properties of graphene microcapsule pitches, and also provides a certain reference for the evaluation of other microcapsule pitch self-healing properties.

Method used

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  • Method for testing and evaluating self-healing property of graphene microcapsule asphalt
  • Method for testing and evaluating self-healing property of graphene microcapsule asphalt
  • Method for testing and evaluating self-healing property of graphene microcapsule asphalt

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Embodiment 1

[0025] A kind of graphene microcapsule asphalt self-healing test evaluation method, the specific operation process of described method is as follows:

[0026] Step 1: Under the test conditions of 25 ° C and 10 Hz, the strain scanning test was carried out on the base asphalt and 5% graphene microcapsule asphalt respectively with an 8 mm flat plate and a dynamic shear rheometer. The dynamic modulus-strain relationship curves of matrix pitch and graphene microcapsule pitch are plotted respectively on the ordinate (such as figure 1 As shown), the intersection point 4.3% of the two relationship curves is the strain threshold, and the value range of the control load is 0-4.3%;

[0027] Step 2: According to the result of Step 1, select 4% strain as the control load, and under the test conditions of 25°C and 10Hz, use an 8mm plate and use a dynamic shear rheometer to continuously load 5% graphene microcapsule asphalt fatigue test (such as figure 2 Shown), test the dynamic modulus o...

Embodiment 2

[0032] A kind of graphene microcapsule asphalt self-healing test evaluation method, the specific operation process of described method is as follows:

[0033] Step 1: Under the test conditions of 25 ° C and 10 Hz, the strain scanning test was carried out on the No. 70 matrix asphalt and 5% graphene microcapsule asphalt respectively by using an 8 mm flat plate and a dynamic shear rheometer, and then the strain was used as the abscissa, The dynamic modulus is the ordinate to plot the dynamic modulus-strain relationship curves of matrix pitch and graphene microcapsule pitch respectively (such as figure 1 As shown), the intersection point 4.3% of the two relationship curves is the strain threshold, and the value range of the control load is 0-4.3%;

[0034] Step 2: According to the result of Step 1, select 3% strain as the control load, and under the test conditions of 25°C and 10Hz, use an 8mm flat plate and use a dynamic shear rheometer to continuously load 5% graphene microcaps...

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Abstract

The invention relates to a graphene microcapsule asphalt self-healing test evaluation method. The method comprises the following steps: firstly, determining a fatigue test control load value range based on matrix asphalt and graphene microcapsule asphalt strain scanning test curve intersection points; then carrying out a fatigue test on the graphene microcapsule asphalt in a continuous loading mode, and recording an initial modulus G0, a termination modulus G1 and a load action frequency N1; then carrying out a fatigue test on the graphene microcapsule asphalt in an intermittent loading mode, and recording an initial modulus G0 ', a termination modulus G1' and a load action frequency N2; and finally, respectively calculating the fatigue curve failure rates in two different loading modes and taking the fatigue curve failure rates as healing indexes to evaluate the self-healing property of the graphene microcapsule asphalt. The method contributes to accurate evaluation of the self-healing property of the graphene microcapsule asphalt, and is of great significance to material design and engineering application of the graphene microcapsule asphalt.

Description

technical field [0001] The invention belongs to the technical field of asphalt self-healing test and evaluation methods, in particular to a graphene microcapsule asphalt self-healing test and evaluation method. Background technique [0002] Graphene microcapsule is a composite structure composed of repair agent as core material, resin material and graphene as wall material. The pitch mixed with an appropriate amount of graphene microcapsules is called graphene microcapsule pitch. The self-healing mechanism of graphene microcapsule asphalt is realized through the rupture of microcapsules and the outflow of repair agent after asphalt damage. Due to the improper selection of the control load value in the existing asphalt self-healing test method, the graphene microcapsules may be broken in advance during the test process, resulting in inaccurate self-healing evaluation results. Therefore, it is necessary to design a self-healing test and evaluation method specifically for gra...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N3/32
CPCG01N3/32G01N2203/0005G01N2203/0025G01N2203/0073G01N2203/0075G01N2203/0676G01N2203/0682
Inventor 单丽岩张恩浩刘爽
Owner HARBIN INST OF TECH