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Polyolefin kettle type reaction constant temperature control method and device

A constant temperature control, polyolefin technology, applied in the direction of temperature control, control/regulation systems, chemical instruments and methods, etc., can solve the problems affecting product melt index product quality index, single-loop control lag, polyolefin product quality impact and other issues

Active Publication Date: 2022-05-27
SHANDONG JINGBO PETROCHEM
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  • Application Information

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Problems solved by technology

[0004] In recent years, with the development of the polyolefin industry, the polyolefin kettle reaction production process has made great progress, and its application in the new product development stage has irreplaceable advantages, but there are still many areas to be improved. In terms of reaction control Constant pressure control is often achieved instead of constant temperature control, which has a great impact on the quality of polyolefin products, and there is a problem of single-loop control lag in the polymerization constant temperature control stage, resulting in large temperature fluctuations during the reaction process, which affects product melt index and molecular weight. and other important product quality indicators

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  • Polyolefin kettle type reaction constant temperature control method and device

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Embodiment Construction

[0035] The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the accompanying drawings in the embodiments of the present invention. However, the present invention is not limited to the following examples. Based on the examples in the present invention, all other examples obtained by those of ordinary skill in the art without creative work fall within the protection scope of the present invention.

[0036] In the process of polyolefin kettle reaction, with the progress of the reaction and the change of material concentration, the temperature in the reaction kettle rises, and the temperature change in the reaction kettle has an impact on the product quality indicators (the molecular weight distribution of the polymer, the change in the melt index and the degree of polymerization, etc. ) has a significant impact, so using the constant temperature control method to control the change of the reaction temp...

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Abstract

The invention provides a polyolefin kettle type reaction constant temperature control method and device.The polyolefin kettle type reaction constant temperature control method comprises the steps that a, the real-time temperature value of a polyolefin reaction kettle is obtained, the real-time temperature value is compared with a preset temperature value, and if the real-time temperature value is different from the preset temperature value, the polyolefin reaction kettle is started; if yes, obtaining a real-time pressure value of the polyolefin reaction kettle according to the real-time temperature value; b) comparing the real-time pressure value with a preset pressure value, and if the real-time pressure value is greater than or equal to the preset pressure value, adjusting the valve position opening degree of the polyolefin reaction kettle to be a minimum value; if the real-time pressure value is smaller than the preset pressure value, the step c) is carried out; and c) according to the real-time pressure value and the preset pressure value of the polyolefin reaction kettle, obtaining the numerical value of the reaction water demand, and adjusting the valve position opening value of the polyolefin reaction kettle according to the numerical value of the reaction water demand. The device is beneficial to realizing constant-temperature automatic accurate control, reducing reaction temperature fluctuation and improving product quality.

Description

technical field [0001] The invention belongs to the field of reaction kettles, and in particular relates to a constant temperature control method and device for a polyolefin kettle type reaction. Background technique [0002] Polyolefin has the advantages of abundant raw materials, easy processing and molding, and excellent comprehensive performance. It is a kind of polymer material with large output and wide application. The polyolefin kettle reaction production process is a self-developed olefin polymerization production method in my country. It has the advantages of low production cost, quick effect, low energy consumption, good economic benefits, less "three wastes" and high safety performance. It is used in my country's oil refineries. widely. [0003] The material of the polyolefin kettle reaction is a mixed material, including monomers and hydrogen. As the polymerization reaction proceeds, the saturated vapor pressure changes. [0004] In recent years, with the devel...

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G05D23/20B01J19/00
CPCG05D23/20B01J19/0013Y02P20/10
Inventor 马丙建闫伟董建永栾波王耀伟
Owner SHANDONG JINGBO PETROCHEM