Water-in-oil type high-internal-phase emulsion carrying bitter substances and preparation method of water-in-oil type high-internal-phase emulsion
A technology of high internal phase emulsion and bitter substance, applied in the field of water-in-oil type high internal phase emulsion carrying bitter substance and preparation thereof, and can solve the problems of low encapsulation rate of double emulsion, low content of bitter substance, poor storage stability and the like , to achieve the effect of improving acceptability, protecting activity and ensuring stability
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[0044] The preparation raw materials in the embodiment and the comparative example are as follows:
[0045] Tea Oil (Green Sea Tea Oil, Nanchang, Jiangxi), Palm Oil (Food Grade, Guangzhou Langfeng), Polyglycerol Ricinoleate (Dahe Food, Zhengzhou, Henan), Wheat Peptide (Jiangzhong, Nanchang, Jiangxi, molecular weight below 1000Da) ), Coconut Oil (Sunshine Coconut Oil, Guangzhou, Guangdong), Flaxseed Oil (Flax Commune, Inner Mongolia, China), Olive Oil (Betis, Spain), Shortening (Citi, Shanghai, China), Collagen Peptides (Jiangsu Peptide Bio, Nanjing, Jiangsu), Coptis chinensis extract (Fufeng Snow, Shaanxi Baoji), traditional Chinese medicine liquid (Jiangxi Provincial Hospital of Traditional Chinese Medicine, Nanchang, Jiangxi).
[0046] In the embodiment and the comparative example, the concentration of the PBS buffer is 5mM, the pH value is 7.0, and the preparation method is as follows:
[0047] Prepare 5mM Na separately 2 HPO 4 solution and 5mM NaH 2 PO 4 solution, 610...
Embodiment 1
[0050] The present embodiment provides a water-in-oil high internal phase emulsion carrying wheat peptides, and its preparation method is as follows:
[0051] (1) dissolve 20g wheat peptide powder in 380g PBS buffer to obtain 400g water phase (wheat peptide mass concentration 5%);
[0052] (2) 47.5g of camellia oil, 47.5g of food-grade palm oil and 5g of polyglycerol ricinoleate were heated and mixed at 70°C to obtain 100g of oil phase;
[0053] (3) transfer the heated oil phase obtained in step (2) into a beaker, and place it in a high-speed disperser. During the process of adding the water phase to the oil phase, the rotational speed is gradually increased by 8000rpm at a rate of 1000rpm per minute. To 11000rpm, after the water phase is completely added, continue to disperse at 11000rpm for 2min to obtain a water-in-oil high internal phase emulsion carrying wheat peptides.
Embodiment 2
[0055] The present embodiment provides a water-in-oil high internal phase emulsion carrying wheat peptides, and its preparation method is as follows:
[0056] (1) 60g wheat peptide powder was dissolved in 340g PBS buffer to obtain 400g water phase (wheat peptide mass concentration 15%);
[0057] (2) 47.5g of camellia oil, 47.5g of food-grade palm oil and 5g of polyglycerol ricinoleate were heated and mixed at 70°C to obtain 100g of oil phase;
[0058] (3) transfer the heated oil phase obtained in step (2) into a beaker, and place it in a high-speed disperser. During the process of adding the water phase to the oil phase, the rotational speed is gradually increased by 8000rpm at a rate of 1000rpm per minute. To 11000rpm, after the water phase is completely added, continue to disperse at 11000rpm for 2min to obtain a water-in-oil high internal phase emulsion carrying wheat peptides.
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