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Ammonium salt filled porous metal spontaneous perspiration composite material and preparation method thereof

A technology of porous metal and composite materials, which is applied to the device and coating of the surface coating liquid, which can solve the problems of unreasonable filling of cooling fluid and mismatching of temperature, and achieve low cost, large decomposition enthalpy, and wide application range wide effect

Active Publication Date: 2022-07-29
XI AN JIAOTONG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0004] In order to overcome the shortcomings of the above-mentioned prior art, the object of the present invention is to provide an ammonium salt-filled porous metal self-sweating composite material and its preparation method, which can effectively solve the problem that the cooling medium cannot be properly filled in the matrix due to the temperature mismatch during the preparation of the composite material. technical difficulties in

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  • Ammonium salt filled porous metal spontaneous perspiration composite material and preparation method thereof
  • Ammonium salt filled porous metal spontaneous perspiration composite material and preparation method thereof

Examples

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Embodiment 1

[0033] A preparation of ammonium salt filled porous metal spontaneous sweating composite material, comprising the following steps:

[0034] 1) Select the porous TC4 alloy with better comprehensive properties among the porous light metal alloys as the matrix material, and select ammonium chloride as its cooling medium.

[0035] 2) The porous TC4 alloy sample was prepared by vacuum sintering. The prepared sample was a disc with a diameter of 35 mm and a thickness of 6 mm, the sample mass was 16.13 g, and the open porosity was 20.2%.

[0036] 3), adopt the repeated negative pressure impregnation method to carry out the preparation of ammonium chloride filling porous TC4 alloy spontaneous perspiration composite material, and the specific preparation process is as follows: 8g of ammonium chloride is mixed with 20ml of deionized water, and stirred at room temperature for 30min to prepare into a supersaturated solution of ammonium chloride. The porous TC4 alloy sample was placed in ...

Embodiment 2

[0040] A preparation of ammonium salt filled porous metal spontaneous sweating composite material, comprising the following steps:

[0041] 1) Select the porous TC4 alloy with better comprehensive properties among the porous light metal alloys as the matrix material, and select ammonium chloride as its cooling medium.

[0042] 2) The porous TC4 alloy sample was prepared by vacuum sintering. The prepared sample was a disc with a diameter of 20 mm and a thickness of 6 mm. The sample mass was 6.44 g and the open porosity was 20.6%.

[0043] 3), adopt the recrystallization method to carry out the preparation of ammonium chloride filling porous TC4 alloy spontaneous perspiration composite material, and the specific preparation process is as follows: 30.1g of ammonium chloride and 50ml of deionized water are mixed in a suction filter bottle, and the temperature is 70 ° C. The solution was stirred for 1 h to prepare a saturated solution of ammonium chloride. The porous TC4 alloy sam...

Embodiment 3

[0045] A preparation of ammonium salt filled porous metal spontaneous sweating composite material, comprising the following steps:

[0046] 1) Select the porous TC4 alloy with better comprehensive properties among the porous light metal alloys as the matrix material, and select the mixed salt of two inorganic salts, ammonium chloride and ammonium bromide, as the cooling medium.

[0047] 2) The porous TC4 alloy sample was prepared by vacuum sintering. The prepared sample was a disc with a diameter of 40 mm and a thickness of 6 mm. The sample mass was 28.01 g and the open porosity was 19.8%.

[0048] 3), adopt the repeated negative pressure impregnation method to carry out the preparation of ammonium chloride / ammonium bromide mixed salt filling porous TC4 alloy spontaneous sweating composite material, and the concrete preparation process is: the ammonium chloride of 7.44g is mixed with the deionized water of 20ml, Stir at room temperature for 30 minutes to prepare a supersaturat...

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Abstract

The invention discloses an ammonium salt filled porous metal spontaneous perspiration composite material and a preparation method thereof. According to the prepared composite material, the ammonium salt accounts for 4.86%-48.8% by volume, the porous metal matrix accounts for 51.2%-95.14% by volume, pores of the porous metal matrix are evenly filled with the ammonium salt, and a good spontaneous perspiration cooling effect is achieved. Meanwhile, the composite material is prepared by adopting three methods, namely a repeated negative pressure impregnation method, a recrystallization method and a recrystallization and repeated negative pressure impregnation combined method.

Description

technical field [0001] The invention belongs to the technical field of preparation of spontaneous perspiration cooling composite materials, in particular to an ammonium salt filled porous metal spontaneous perspiration composite material and a preparation method thereof. Background technique [0002] Spontaneous perspiration cooling composite material is to fill the cooling medium into the porous matrix. When the material is heated, the cooling medium in the composite material undergoes phase change or decomposition, and then absorbs a large amount of heat to achieve the purpose of cooling the matrix. As far as the currently applied spontaneous perspiration cooling composite materials are concerned, the spontaneous perspiration cooling composite materials based on refractory metals have problems such as high density and low temperature brittleness, while the spontaneous perspiration cooling composite materials based on inorganic non-metallic materials are also brittle. Probl...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B05D7/14B05D7/24B05D1/18
CPCB05D7/14B05D7/24B05D1/18B05D2202/30B05D2202/25B05D2202/15
Inventor 王红洁王泽铭彭康苏磊戴志伟
Owner XI AN JIAOTONG UNIV
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