Corrosion-resistant aluminum conductive material and process for producing the same
A conductive material and manufacturing method technology, applied in metal material coating process, electrolytic capacitor, hybrid capacitor electrode, etc., to achieve the effect of excellent corrosion resistance
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Embodiment 1
[0036] Aluminum plate (JIS H 4000; A5052) with a thickness of 0.5 mm is degreased, followed by zincate treatment, and electroplating nickel treatment (Ni electroplating treatment) to form a nickel-plated film with a thickness of 2 μm on the surface, followed by electroplating gold (Au plating treatment), a gold-plated film with a thickness of 1 μm was formed.
[0037] Next, the obtained plated aluminum plate was kept in hot water (pH: 5.5, phosphate ion concentration (P): 2 ppm, silicate ion concentration (Si) 1 ppm) at 100°C for 30 minutes to perform hot water treatment. , extracted from hot water and dried to produce the corrosion-resistant aluminum plate (corrosion-resistant aluminum conductive material) of Example 1.
[0038] Cut out a test piece with a length of 50 mm × a width of 50 mm from the corrosion-resistant aluminum plate obtained in Example 1, make the scanning potential 0 to 1000 mV vs.Ag / AgCl, and polarize the potential of the test piece with respect to the sil...
Embodiment 2
[0043] In 1 L of 1-methyl-2-pyrrolidone containing 10 g of carbon black with an average particle diameter of 0.5 μm and 2 g of polyvinylidene fluoride, an aluminum plate degreased in the same manner as in Example 1 was arranged as an anode, and a carbon electrode was also arranged as an anode. For the cathode, a voltage of 10 V was applied between these electrodes for 1 minute to perform carbon electrophoresis, and a carbon film with a thickness of 1 μm was formed on the surface of the aluminum plate.
[0044] Next, the obtained aluminum plate after the carbon electrophoresis treatment was held in steam at 120° C. for 30 minutes to perform steam treatment, and the corrosion-resistant aluminum plate (corrosion-resistant aluminum conductive material) of Example 2 was produced.
[0045] About the obtained anti-corrosion aluminum plate of Example 2, it carried out similarly to the said Example 1, the corrosion resistance evaluation test, the electrical conductivity evaluation test,...
Embodiment 3
[0048] Carbon black with an average particle diameter of 0.5 μm and polyvinylidene fluoride were mixed with 1-methyl-2-pyrrolidone at a ratio of 1:1 to prepare a coating liquid, and the coating liquid was applied on the same surface as in Example 1 above. The surface of the aluminum plate degreased in the same manner was subjected to carbon coating treatment, followed by drying at 200° C. for 2 minutes to form a carbon-containing film with a thickness of 1 μm on the surface of the aluminum plate.
[0049] Next, the obtained carbon-coated aluminum plate was kept in steam at 120° C. for 30 minutes to perform a steam treatment, and the corrosion-resistant aluminum plate (corrosion-resistant aluminum conductive material) of Example 3 was produced.
[0050] About the obtained anti-corrosion aluminum plate of Example 3, it carried out similarly to said Example 1, the corrosion resistance evaluation test, the electrical conductivity evaluation test, and comprehensive evaluation were p...
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Abstract
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