Photosensitive resin composition and resin plate for flexography
a technology of which is applied in the field of photosensitive resin composition and resin plate for flexography, can solve the problems of not being able to be extracted with water or aqueous solvent, being highly toxic to the human body, and being unfavorable from the viewpoint of the working environmen
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production example 1
[0043] In a four-neck flask equipped with a stirrer, a thermometer, a condenser, a dropping funnel and a nitrogen gas-introducing pipe, 100 parts by weight of methyl ethyl ketone was placed, and the temperature thereof was raised to 75.degree. C. Then, 2.5 parts by weight of a methyl ethyl ketone solution containing 20 wt % of azobis-2-methylbutyronitrile was poured thereinto while blowing nitrogen gas therein. Subsequently, a previously prepared monomer mixture consisting of 5.1 parts by weight of acrylic acid, 54.8 parts by weight of methyl methacrylate and 40.1 parts by weight of ethyl acrylate was added dropwise for 2 hours. The temperature in the flask during dropping was maintained at the reflux temperature of methyl ethyl ketone. After termination of dropping, the temperature was maintained at the same temperature for 2 hours. Then, 5 parts by weight of a methyl ethyl ketone solution containing 20 wt % of azobis-2-methylbutyronitrile was poured thereinto, and the resulting so...
production example 2
[0044] In a four-neck flask equipped with a stirrer, a thermometer, a condenser, a dropping funnel and a nitrogen gas-introducing pipe, 100 parts by weight of methyl ethyl ketone was placed, and the temperature thereof was raised to 75.degree. C. Then, 6.25 parts by weight of a methyl ethyl ketone solution containing 20 wt % of azobis-2-methylbutyronitrile was poured thereinto while blowing nitrogen gas therein. Subsequently, a previously prepared monomer mixture consisting of 11.5 parts by weight of acrylic acid, 62.4 parts by weight of methyl methacrylate and 26.1 parts by weight of ethyl acrylate was added dropwise for 2 hours. The temperature in the flask during dropping was maintained at the reflux temperature of methyl ethyl ketone. After termination of dropping, the temperature was maintained at the same temperature for 2 hours. Then, 5 parts by weight of a methyl ethyl ketone solution containing 20 wt % of azobis-2-methylbutyronitrile was poured thereinto, and the resulting ...
production example 3
[0045] In a four-neck flask equipped with a stirrer, a thermometer, a condenser, a dropping funnel and a nitrogen gas-introducing pipe, 100 parts by weight of methyl ethyl ketone was placed, and the temperature thereof was raised to 75.degree. C. Then, 1 part by weight of a methyl ethyl ketone solution containing 20 wt % of azobis-2-methylbutyronitrile was poured thereinto while blowing nitrogen gas therein. Subsequently, a previously prepared monomer mixture consisting of 13.5 parts by weight of acrylic acid, 83.8 parts by weight of methyl methacrylate and 2.7 parts by weight of ethyl acrylate was added dropwise for 2 hours. The temperature in the flask during dropping was maintained at the reflux temperature of methyl ethyl ketone. After termination of dropping, the temperature was maintained at the same temperature for 2 hours. Then, 5 parts by weight of a methyl ethyl ketone solution containing 20 wt % of azobis-2-methylbutyronitrile was poured thereinto, and the resulting solut...
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Abstract
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