An apparatus for filling a chlorosilane resin adsorption column with resin

CN115944949BActive Publication Date: 2026-09-11XINJIANG DAQO NEW ENERGY CO LTD
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Patent Information

Application Number
CN202310032605.8
Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
Filing Date
2023-01-10
Publication Date
2026-09-11
Estimated Expiration
2043-01-10

AI Technical Summary

Technical Problem

在此过程中,由于氯硅烷与树脂中残留水分反应放热,氯硅烷通入速度较慢,反应热不能及时带走,会导致树脂局部过热,出现树脂粉化,活性基团流失导致树脂失活,甚至出现安全事故;二为树脂通过人孔直接倒入氯硅烷树脂吸附柱;在此过程中,由于氯硅烷汽化分压较低,极易汽化与空气中水分反应生成氯化氢污染环境,同时对操作人员产生伤害;另外,树脂密度较氯硅烷小,树脂浮在氯硅烷表面不能充分反应,存在集聚放热的风险;并且,直接倾倒过程中也会将空气带入系统,对生产造成危害;三为采用气力输送的方式将树脂送入到氯硅烷树脂吸附柱

Benefits of technology

[0023] It can improve the efficiency and safety of resin filling, and reduce the labor intensity and danger for operators.

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Abstract

The present application relates to the technical fields of polysilicon production equipment, and particularly relates to a device for filling resin into a chlorosilane resin adsorption column, which comprises a support frame, a resin container, a filter screen, a pneumatic air extractor and a resin drying tank; the support frame is provided with traveling wheels; the resin container is arranged on the support frame; the lower end of the resin container is provided with a discharging port; the upper part of the resin container is provided with a feeding groove; the feeding groove is located on one side of the resin container; the filter screen is arranged at the connecting part of the feeding groove and the resin container; the inlet end of the pneumatic air extractor is connected to the discharging port through a joint one; the outlet end of the pneumatic air extractor is connected to one end of a resin conveying hose through a joint two; the other end of the resin conveying hose is connected to the guide of the resin drying tank; the resin drying tank is higher than the resin container; the air nozzle joint of the pneumatic air extractor is communicated with a gas pressure increasing device through a nitrogen pipe. The present application can improve the efficiency and safety of resin filling, and reduce the labor intensity and danger of the operator.
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Description

Technical Field

[0001] This invention relates to the field of polycrystalline silicon production equipment technology, and more particularly to an apparatus for filling a chlorosilane resin adsorption column with resin. Background Technology

[0002] There are three main methods for loading chlorosilane adsorption resin in the polysilicon production process. The first method involves loading the resin into a chlorosilane resin adsorption column, purging it with nitrogen, and then introducing chlorosilane into the bottom of the column. During this process, because the reaction between chlorosilane and residual moisture in the resin is exothermic, the slow rate of chlorosilane introduction means the heat cannot be carried away in time, leading to localized overheating of the resin, resin pulverization, loss of active groups resulting in resin deactivation, and even safety accidents. The second method involves pouring the resin directly into the chlorosilane resin adsorption column through a manhole. In this process, because chlorosilane has a low vaporization partial pressure, it easily vaporizes and reacts with moisture in the air to generate hydrogen chloride, polluting the environment and harming operators. Furthermore, the resin has a lower density than chlorosilane, and the resin floating on the surface of the chlorosilane cannot react fully, posing a risk of agglomeration and exothermic reactions. Direct pouring also introduces air into the system, jeopardizing production. The third method involves using pneumatic conveying to deliver the resin into the chlorosilane resin adsorption column. During pneumatic conveying, a certain amount of chlorosilane needs to be loaded into the chlorosilane resin adsorption column. In order to ensure that the resin and chlorosilane can fully contact each other, a submersible insertion tube method is required, which requires high nitrogen pressure. Moreover, the pneumatic conveying distance is long and the flow rate is fast, which causes significant wear on the resin. The resin cannot form a uniform dispersion flow in the pipeline, and blockage is very likely to occur during solid phase conveying. Summary of the Invention

[0003] In view of this, the present invention provides an apparatus for filling a chlorosilane resin adsorption column with resin, the main purpose of which is to improve the efficiency and safety of resin filling and reduce the labor intensity and danger of operators.

[0004] To achieve the above objectives, the present invention mainly provides the following technical solutions:

[0005] An embodiment of the present invention provides an apparatus for filling a chlorosilane resin adsorption column with resin, comprising: a support frame, a resin container, a filter screen, a pneumatic exhaust fan, and a resin drying tank;

[0006] The support frame is equipped with wheels for supporting its movement;

[0007] The resin container is fixedly mounted on the support frame;

[0008] The lower end of the resin container has a discharge port; the discharge port has a conical structure.

[0009] A feed trough is fixedly provided on the upper part of the resin container; the feed trough is located on one side of the resin container; the bottom of the feed trough is inclined towards the resin container.

[0010] The filter screen is disposed at the connection between the feed trough and the resin container, and is used to filter the material entering the resin container;

[0011] The inlet end of the pneumatic exhaust fan is connected to the discharge port via a connector.

[0012] The outlet end of the pneumatic exhaust fan is connected to one end of the resin delivery hose via connector two; the other end of the resin delivery hose is connected to the drain of the resin drying tank; the resin drying tank is positioned higher than the resin container.

[0013] The air nozzle of the pneumatic exhaust fan is connected to the gas pressurization device via a nitrogen pipe.

[0014] The nitrogen pipe is equipped with a nitrogen valve for regulating the flow rate of the nitrogen pipe.

[0015] Furthermore, the first connector is a quick connector.

[0016] Furthermore, the second connector is a quick connector.

[0017] Furthermore, the pneumatic exhaust fan is a bladeless pneumatic conveyor.

[0018] Furthermore, the top of the resin drying tank has a feeding port;

[0019] The top of the resin drying tank has a vent.

[0020] The bottom of the resin drying tank has a material outlet for conveying resin to the chlorosilane resin adsorption column.

[0021] Furthermore, a handrail is fixedly provided on the support frame.

[0022] By employing the above technical solution, the apparatus of the present invention for filling a chlorosilane resin adsorption column with resin has at least the following advantages:

[0023] It can improve the efficiency and safety of resin filling, and reduce the labor intensity and danger for operators.

[0024] The above description is merely an overview of the technical solution of the present invention. In order to better understand the technical means of the present invention and to implement it in accordance with the contents of the specification, the preferred embodiments of the present invention are described in detail below with reference to the accompanying drawings. Attached Figure Description

[0025] Figure 1This is a schematic diagram of an apparatus for filling a chlorosilane resin adsorption column, provided as an embodiment of the present invention.

[0026] As shown in the figure:

[0027] 1 is the support frame, 1-1 is the traveling wheel, 2 is the resin container, 3 is the filter screen, 4 is the pneumatic exhaust fan, 5 is the resin drying tank, 5-1 is the feeding port, 5-2 is the vent port, 6 is the feeding trough, 7 is the gas pressurization device, 8 is the nitrogen pipe, and 9 is the resin delivery hose. Detailed Implementation

[0028] To further illustrate the technical means and effects adopted by the present invention to achieve the intended purpose, the specific embodiments, structures, features, and effects according to the present invention will be described in detail below with reference to the accompanying drawings and preferred embodiments. In the following description, different "embodiments" or "embodiments" do not necessarily refer to the same embodiment. Furthermore, specific features, structures, or characteristics in one or more embodiments can be combined in any suitable form.

[0029] like Figure 1 As shown, an embodiment of the present invention provides an apparatus for filling a chlorosilane resin adsorption column with resin, comprising: a support frame, a resin container, a filter screen, a pneumatic exhaust fan, and a resin drying tank; the support frame is a frame structure used to support the resin container. The support frame can be welded or fastened from shaped steel. The support frame is equipped with wheels for moving the support frame. Preferably, in this embodiment, a handrail is fixedly provided on the support frame to facilitate operation of the support frame.

[0030] The resin container is fixedly mounted on a support frame for temporary storage of resin to be filled. The lower end of the resin container has a discharge port; the discharge port has a conical structure so that the resin gathers towards the discharge port under its own weight.

[0031] A feed trough is fixedly provided on the upper part of the resin container; the feed trough is located on one side of the resin container; the bottom of the feed trough is inclined towards the resin container to facilitate the operator to fill the resin from the feed trough.

[0032] The filter screen is installed at the connection between the feed trough and the resin container to filter the material entering the resin container and prevent clumps of resin and other impurities from entering.

[0033] The inlet of the pneumatic exhaust fan is connected to the discharge port via connector one; preferably, connector one is a quick connector for quick connection and convenient resin filling. The outlet of the pneumatic exhaust fan is connected to one end of the resin delivery hose via connector two; preferably, connector two is a quick connector for quick connection and convenient resin filling. The other end of the resin delivery hose is connected to the drain valve of the resin drying tank; the drain valve is located at the top of the resin drying tank to guide the resin into the resin drying tank. The resin drying tank is positioned higher than the resin container to transport the resin in the resin container to the higher resin drying tank. In this embodiment, preferably, the top of the resin drying tank has a feed port for adding resin as a backup feed port. The top of the resin drying tank has a vent; the bottom of the resin drying tank has a material outlet for conveying resin to the chlorosilane resin adsorption column.

[0034] The pneumatic exhaust fan's nozzle connector is connected to a gas pressurization device via a nitrogen pipe to deliver resin using high-pressure nitrogen, reducing resin contact with air. The pneumatic exhaust fan is a bladeless pneumatic conveyor. A nitrogen valve is installed on the nitrogen pipe to regulate the nitrogen flow rate.

[0035] An embodiment of the present invention provides an apparatus for filling a chlorosilane resin adsorption column with resin, which can improve the efficiency and safety of resin filling and reduce the labor intensity and danger of operators.

[0036] An embodiment of the present invention provides an apparatus for filling a chlorosilane resin adsorption column with resin. By filling the adsorption column with resin through a resin drying tank, the dryness of the resin and the environmental stability of the resin can be guaranteed.

[0037] Existing resin drying tanks are relatively tall and numerous; an embodiment of the present invention proposes a device for filling resin into a chlorosilane resin adsorption column, which can easily move the support frame to the vicinity of the resin drying tank for resin addition.

[0038] The pneumatic exhaust fan housing contains an inlet chamber, a swirling chamber, and an exhaust chamber, all of which are interconnected. An inlet channel is provided on the housing, connecting to an air nozzle connector. Compressed gas is injected into the swirling chamber through the inlet channel, forming a high-speed swirling current. A negative pressure zone is created within the swirling chamber, where resin draws the gas in from the inlet chamber under this negative pressure. After mixing with the high-speed compressed gas in the swirling chamber, the mixture is discharged from the exhaust chamber.

[0039] To further clarify, while the terms "first," "second," etc., may be used herein to describe various elements, these terms should not limit the elements. These terms are used only to distinguish one element from another. For example, a first element may be referred to as a second element, and similarly, a second element may be referred to as a first element; these terms are used only to distinguish one element from another. This does not depart from the scope of the exemplary embodiments. Similarly, "element one," "element two," and so on do not represent the order of elements; these terms are used only to distinguish one element from another. As used herein, the term "and / or" includes any and all combinations of one or more associated listed items.

[0040] In the description of this invention, unless otherwise explicitly specified and limited, the terms "installation," "connection," "linking," and "fixing" should be interpreted broadly. For example, they can refer to a fixed connection, a detachable connection, or an integral part; they can refer to a mechanical connection or an electrical connection; they can refer to a direct connection or an indirect connection through an intermediate medium; they can refer to the internal communication of two components or the interaction between two components. Those skilled in the art can understand the specific meaning of the above terms in this invention based on the specific circumstances.

[0041] All standard parts used in this invention can be purchased from the market, and irregular parts can be customized according to the description and drawings. The specific connection methods of each part adopt conventional methods such as bolts, rivets, and welding that are mature in the prior art. The machinery, parts and equipment adopt conventional models in the prior art, and the circuit connection adopts conventional connection methods in the prior art, which will not be described in detail here.

[0042] The above description is merely a preferred embodiment of the present invention and is not intended to limit the present invention in any way. Any simple modifications, equivalent changes, and alterations made to the above embodiments based on the technical essence of the present invention shall still fall within the scope of the technical solution of the present invention.

Claims

1. An apparatus for filling a chlorosilane resin adsorption column with resin, characterized in that, Includes: support frame, resin container, filter screen, pneumatic exhaust fan and resin drying tank; The support frame is equipped with wheels for supporting its movement; The resin container is fixedly mounted on the support frame; The lower end of the resin container has a discharge port; the discharge port has a conical structure. A feed trough is fixedly provided on the upper part of the resin container; the feed trough is located on one side of the resin container; the bottom of the feed trough is inclined towards the resin container. The filter screen is disposed at the connection between the feed trough and the resin container, and is used to filter the material entering the resin container; The inlet end of the pneumatic exhaust fan is connected to the discharge port via a connector. The outlet end of the pneumatic exhaust fan is connected to one end of the resin delivery hose via connector two; the other end of the resin delivery hose is connected to the drain of the resin drying tank; the resin drying tank is positioned higher than the resin container. The air nozzle of the pneumatic exhaust fan is connected to the gas pressurization device via a nitrogen pipe. The nitrogen pipe is equipped with a nitrogen valve for regulating the flow rate of the nitrogen pipe.

2. The apparatus for packing resin into a chlorosilane resin adsorption column according to claim 1, characterized in that, The first connector is a quick connector.

3. The apparatus for packing resin into a chlorosilane resin adsorption column according to claim 1, characterized in that, The second connector is a quick connector.

4. The apparatus for packing resin into a chlorosilane resin adsorption column according to claim 1, characterized in that, The pneumatic exhaust fan is a bladeless pneumatic conveyor.

5. The apparatus for packing resin into a chlorosilane resin adsorption column according to claim 1, characterized in that, The top of the resin drying tank has a feeding port; The top of the resin drying tank has a vent. The bottom of the resin drying tank has a material outlet for conveying resin to the chlorosilane resin adsorption column.

6. The apparatus for packing resin into a chlorosilane resin adsorption column according to claim 1, characterized in that, Handrails are fixedly installed on the support frame.

Citation Information

Patent Citations

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    CN101592169A

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    CN110613955A

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