一种质子交换膜燃料电池催化剂及其制备方法

By combining atmospheric ball milling with pulverization and loading processes, the problems of uncontrollable functionalization of carbon materials and complex preparation of supported catalysts were solved. This achieved uniform modification of functional groups on the surface of carbon materials and uniform dispersion of active components, making it suitable for industrial production.

CN116190684BActive Publication Date: 2026-07-17STATE POWER INVESTMENT CORP HYDROGEN ENERGY CO LTD +1

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
STATE POWER INVESTMENT CORP HYDROGEN ENERGY CO LTD
Filing Date
2023-03-14
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

In existing technologies, the degree of surface functionalization of carbon materials treated by ozone is uncontrollable and the equipment is complex. The preparation process of supported catalysts is cumbersome and polluting, making it difficult to achieve large-scale production and uniform loading.

Method used

The surface of carbon materials is modified by atmospheric ball milling. Combining pulverization, surface modification and loading processes, ozone is used to react gently with carbon materials in the ball mill jar to form a loaded metal precursor salt solution under negative pressure, which simplifies the preparation process.

Benefits of technology

The proportion of oxygen-containing functional groups on the surface of carbon materials is increased, achieving uniform dispersion and pore loading of active components, simplifying the preparation process, reducing costs, and making it suitable for industrial applications.

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Abstract

本发明属于质子交换膜燃料电池技术领域,具体涉及一种质子交换膜燃料电池催化剂及其制备方法。本发明实施例提供的质子交换膜燃料电池催化剂的制备方法,包括以下步骤:(1)将碳材料和球磨珠放入球磨罐内,向球磨罐内通入含有臭氧的气体后进行球磨,得到表面功能化的碳材料;(2)将金属前驱体盐溶液通过球磨罐的进气口送入球磨罐内,关闭进气口继续球磨,球磨结束后进行后处理,获得负载型催化剂。该方法利用气氛球磨的方法对碳材料表面进行改性,促进球磨罐内臭氧与碳材料的温和反应,将碳材料表面进行功能化,能提高并调控碳材料表面的含氧官能团比例,并将粉碎工艺、表面改性工艺和担载工艺结合为一个工艺,能够大幅度节约时间成本。
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