单晶硅的培育方法

By controlling the heat generation ratio Qd/Qu of the heating section during the cultivation of single-crystal silicon, the temperature of the silicon melt surface is reduced, solving the problems of large evaporation of volatile dopants and dislocation, thus achieving efficient dopant addition and cultivation of low resistivity single-crystal silicon.

CN116324050BActive Publication Date: 2026-07-17SUMCO CORP

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
SUMCO CORP
Filing Date
2021-07-30
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

In existing technologies for cultivating monocrystalline silicon, the evaporation of volatile dopants is large, resulting in a poor hit rate of the target resistivity of monocrystalline silicon. Furthermore, the formation of a solidification layer in the high-pressure chamber can lead to dislocation problems.

Method used

By preventing the formation of a solidified layer on the surface of the molten silicon, and by heating the crucible with a lower heating section generating more heat than the upper heating section, the temperature of the liquid surface is reduced, thereby suppressing the evaporation of volatile dopants. Furthermore, by controlling the heating ratio Qd/Qu within a specific range, reliable addition of dopants is ensured.

Benefits of technology

It effectively suppressed the evaporation of volatile dopants, reduced the deviation of evaporation amount, improved the target resistivity hit rate of single crystal silicon, and avoided the occurrence of dislocation, thus ensuring the reliability of the doping process.

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Abstract

本发明提供一种单晶硅的培育方法,其利用单晶硅培育装置,通过切克劳斯基法培育单晶硅,该单晶硅培育装置具备:腔室;坩埚;加热部,对容纳于坩埚中的硅熔液进行加热;及提拉部,使籽晶与硅熔液接触之后将其提拉,加热部具备对坩埚的上部进行加热的上加热部和对坩埚的下部进行加热的下加热部,单晶硅的培育具有:掺杂剂添加工序(S4),向硅熔液中添加挥发性掺杂剂;及提拉工序(S5),在掺杂剂添加工序(S4)之后提拉单晶硅,在掺杂剂添加工序(S4)中,不在硅熔液的液面上形成固化层,而以下加热部的发热量(Qd)和上加热部的发热量(Qu)成为Qd>Qu的方式对坩埚进行加热。
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