一种高氮钛粉和高性能钛制件及其制备方法

By generating a nitride film on the surface of titanium alloy powder through planetary ball milling and powder blank hot deformation technology, the problem of uniform distribution of high-nitrogen titanium powder was solved, and high-performance titanium alloy parts were prepared, which significantly improved their mechanical properties and reduced production costs.

CN116441533BActive Publication Date: 2026-07-17UNIV OF SCI & TECH BEIJING

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
UNIV OF SCI & TECH BEIJING
Filing Date
2022-11-04
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Existing heat treatment nitriding methods consume a lot of energy, resulting in high production costs for high-performance titanium alloy parts. Furthermore, conventional methods cannot achieve a uniform distribution of high nitrogen content, which affects the mechanical properties of titanium alloys.

Method used

A nitride film is generated on the surface of titanium alloy powder by planetary ball milling. High-nitrogen titanium powder is prepared by controlling the ball milling process parameters and nitrogen pressure through powder blank hot deformation technology. High-performance titanium alloy parts are then prepared by cold isostatic pressing and high-temperature hot extrusion.

Benefits of technology

Uniform nitriding of high-nitrogen titanium powder was achieved, resulting in titanium alloy parts with fine grains and equiaxed α microstructure with dispersed β phase. This significantly improved their room temperature mechanical properties and reduced production costs.

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Abstract

一种高氮钛粉和高性能钛制件及其制备方法,该高氮钛粉的制备方法采用行星球磨氮化钛及钛合金粉末,包括以下步骤:选择钛及钛合金粉末作为原料粉末;将该原料粉末置于球磨罐中,加入磨球并选择性加入硬脂酸、航空煤油或酒精作为球磨介质,将球磨罐抽真空后充入氮气气氛,进行行星球磨获得氮化粉末;将获得的该氮化粉末进行真空干燥得到干燥粉末;以及对该干燥粉末进行分级筛分。本发明还提供了高性能钛合金制件的制备方法及其制品。本发明在行星球磨作用下使得钛合金粉末与罐内氮气发生反应,通过控制球磨工艺参数使钛粉表面生成氮化膜,采用冷压烧结获得氮元素均匀分布的稳定组织,实现了粉末坯高温热变形,最终获得氮固溶强化的高性能钛合金。
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