一种改善定向凝固初期籽晶氧化引起凝固缺陷形成的方法

By adjusting the position and time control of the water-cooled plate in the directional solidification furnace, the solidification defect problem caused by seed crystal oxidation was solved, which simplified the process, reduced costs, and improved the success rate of preparing single-crystal superalloys.

CN116460278BActive Publication Date: 2026-07-17XIANGTAN UNIV +1

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
XIANGTAN UNIV
Filing Date
2023-05-24
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

In the preparation of single-crystal superalloys, the oxidation of the seed crystal tip leads to solidification defects, resulting in complicated processes and high costs, which limits the application of the seed crystal method in industrial production.

Method used

By adjusting the position of the water-cooled plate in the directional solidification furnace, the temperature field and microstructure evolution of the seed crystal can be controlled, preventing the seed crystal tip from oxidizing at high temperatures. After the melt is poured, the position of the water-cooled plate is adjusted and the settling time is extended to ensure the microstructure of the seed crystal in the remelting zone and reduce solidification defects.

Benefits of technology

It simplifies the process, reduces costs, increases the success rate of single crystal preparation, effectively improves solidification defects caused by seed crystal oxidation, and is suitable for industrial production.

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Abstract

本发明公开一种改善定向凝固初期籽晶氧化引起凝固缺陷形成的方法,包括将籽晶、模壳安装到定向凝固炉的水冷板上,调节水冷板位置对模壳预加热,熔融母合金浇注到模壳内,调节水冷板位置保温回熔籽晶,抽拉获得单晶铸件等步骤。本发明在明确定向凝固过程中温度场和显微组织演化的基础上提出改善籽晶氧化的技术方案。通过调节水冷板的位置保证加热过程中模壳上部达到预设温度,且籽晶仍处于较低温度,以避免籽晶在高温下发生明显氧化,改善单晶制备过程中籽晶氧化引起凝固缺陷形成的问题;同时能保证定向凝固过程中不出现未完全熔解的破碎枝晶导致定向凝固过程中形成杂晶等凝固缺陷,提高籽晶法制备单晶的成功率,工艺简单、成本低、成功率高。
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