一种高取向晶面氢氧化镁阻燃剂的制备方法

This method prepares highly oriented magnesium hydroxide flame retardant via a one-step gas-liquid heterogeneous reaction, solving the problem of poor dispersibility of magnesium hydroxide in polymer materials. It achieves a high-purity, low-cost preparation method that is suitable for industrial production.

CN116715259BActive Publication Date: 2026-07-17SHENYANG INSTITUTE OF CHEMICAL TECHNOLOGY

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
SHENYANG INSTITUTE OF CHEMICAL TECHNOLOGY
Filing Date
2023-05-15
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Existing magnesium hydroxide flame retardants exhibit poor dispersibility when added to polymer materials, affecting the mechanical properties of composite materials. Furthermore, traditional preparation methods are cumbersome and costly, hindering large-scale production.

Method used

A one-step gas-liquid heterogeneous reaction was adopted to prepare a highly oriented magnesium hydroxide flame retardant by controlling the bubbling frequency and volume of ammonia molecules, avoiding the use of directing agents and viscosity reducers, and controlling the process conditions for precipitation reaction and subsequent treatment.

Benefits of technology

The controlled growth of magnesium hydroxide crystals has been achieved, resulting in products with high purity and uniform particle size. This simplifies the preparation process, reduces production costs, and facilitates industrial production.

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Abstract

一种高取向晶面氢氧化镁阻燃剂的制备方法,涉及一种阻燃剂的制备方法,本发明以气液非均相反应为基础,通过调节气态原料的进料参数,强化其与镁盐溶液的有效接触,调控氢氧化镁生长基元在晶面的生长速度,实现低温常压下对氢氧化镁阻燃剂(001)晶面的选择性调控,制备具有高取向(001)晶面氢氧化镁阻燃剂。本发明无需添加任何诱导剂,利用一步气液非均相反应获得形貌规则、分散性良好、高取向(001)晶面的氢氧化镁阻燃剂,可有效克服传统两步法制备氢氧化镁生产工艺流程长、产品结晶度低、(001)晶面取向低和晶体缺陷可控性差的难题。制备的氢氧化镁产物易于分离,后续处理过程简单,产品纯度高于98%。
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