A fixing hair composition, a method for preparing the same and use thereof

Abstract

The application discloses a color-fixing hair composition, a preparation method and application thereof, and belongs to the field of hair care products. The color-fixing hair composition comprises the following components: amodimethicone, polyquaternium, cocamide MEA, lactobacillus fermentation lysate, tuber melanosporum extract, hydroxyethyl urea and glycyrrhizic acid dipotassium. The application combines amodimethicone, cocamide MEA, polyquaternium, lactobacillus fermentation lysate, tuber melanosporum extract and glycyrrhizic acid dipotassium, and the composition with a significant color-fixing effect is prepared through the combined action of the components, and can be used in hair washing and conditioning products with a color-fixing effect.

Description

Technical Field

[0001] This invention relates to the field of daily chemical product technology, specifically to a color-fixing hair composition, its preparation method, and its application. Background Technology

[0002] With rising living standards and a growing pursuit of beauty, hair dyeing is becoming increasingly popular among consumers. However, existing perming and dyeing products contain a significant amount of chemicals, which damage the hair cuticle. After dyeing, hair becomes more fragile, resulting in color fading with each wash. Over time, the hair color may change noticeably, such as turning yellow.

[0003] Existing hair care products mainly focus on nourishing, softening, oil control, and dandruff removal, with very little research on color-fixing products and related aspects. Therefore, the purpose of this invention is to develop a composition with color-fixing effects for use in hair care products. Summary of the Invention

[0004] To address the shortcomings of existing technologies, the present invention aims to provide a color-fixing hair composition, its preparation method, and its application.

[0005] The objective of this invention is achieved through the following technical solution:

[0006] The present invention provides a color-fixing hair composition comprising the following components: amino-terminated polydimethylsiloxane, polyquaternium salt, cocamidomethyl MEA, lactobacillus fermentation lysate, white truffle extract, hydroxyethyl urea, and dipotassium glycyrrhizate.

[0007] As a preferred embodiment, the polyquaternium salt includes polyquaternium salt-7 and polyquaternium salt-10.

[0008] As a preferred embodiment, the hair-fixing composition comprises the following components in parts by weight: 1-5 parts of water / ammonia-terminated polydimethylsiloxane / tridecyl alcohol polyether-5 / glycerin / tridecyl alcohol polyether-10 / polydimethylsiloxane / trimethylsiloxysilicate / phenoxyethanol / acetic acid, 0.5-2.5 parts of cocamidomethyl MEA / glycerin, 1-2 parts of water / polyquaternium-7 / sodium benzoate, 0.4-0.8 parts of polyquaternium-10 / sodium chloride / water, 0.3-0.5 parts of water / hydroxyethyl urea, 0.1-0.5 parts of lactobacillus fermentation lysate / white truffle extract / capryloyl hydroxamic acid / caprylyl glycol / glycerin, and 0.01-0.05 parts of dipotassium glycyrrhizate.

[0009] As a preferred embodiment, the weight ratio of water / ammonia-terminated polydimethylsiloxane / tetranol polyether-5 / glycerol / tetranol polyether-10 / polydimethylsiloxane / trimethylsiloxysilicate / phenoxyethanol / acetic acid to cocamidomethylMEA / glycerol is 2:1.

[0010] The present invention also provides the application of the aforementioned color-fixing hair composition in shampoo and hair care products.

[0011] As a preferred embodiment, the hair care products include shampoo, conditioner, and hair mask.

[0012] The present invention also provides a color-fixing shampoo, comprising the aforementioned color-fixing hair composition, and further comprising at least one of a solvent, surfactant, pH adjuster, humectant, fragrance, preservative, and chelating agent.

[0013] As a preferred embodiment, the solvent is water;

[0014] The surfactant is selected from sodium laureth sulfate, cocamidopropyl betaine, and sodium cocoyl methyl taurate taurate.

[0015] The pH adjuster is selected from citric acid;

[0016] The humectant is selected from panthenol;

[0017] The fragrance agent is selected from flavorings;

[0018] The preservative is selected from phenoxyethanol and sodium benzoate;

[0019] The chelating agent is selected from disodium EDTA.

[0020] As a preferred embodiment, the components include the following parts by weight:

[0021] 1-5 parts of water / ammonia-terminated polydimethylsiloxane / tridecyl alcohol polyether-5 / glycerin / tridecyl alcohol polyether-10 / polydimethylsiloxane / trimethylsiloxysilicate / phenoxyethanol / acetic acid, 0.5-2.5 parts of cocamidomethyl MEA / glycerin, 1-2 parts of water / polyquaternium-7 / sodium benzoate, 0.4-0.8 parts of polyquaternium-10 / sodium chloride / water, 0.3-0.5 parts of water / hydroxyethyl urea, 0.1-0.5 parts of lactobacillus fermentation lysate / white truffle extract / capryloyl hydroxamic acid / caprylyl glycol / glycerin, 0.01-0.05 parts of dipotassium glycyrrhizate, 10-20 parts of surfactant, 0.1-0.5 parts of pH adjuster, 0.1-0.2 parts of humectant, 0-0.5 parts of fragrance, 0-1 part of preservative, 0-0.1 parts of chelating agent, and solvent to bring the total to 100 parts.

[0022] The present invention also provides a method for preparing the aforementioned color-fixing shampoo, characterized by comprising the following steps:

[0023] The components of the aforementioned color-fixing hair composition, along with moisturizers, emollients, thickeners, chelating agents, fragrances, and preservatives, are weighed out in proportion and added to a solvent. The mixture is then stirred until homogeneous to obtain the color-fixing shampoo.

[0024] Compared with the prior art, the present invention has the following beneficial effects:

[0025] This invention combines amino-terminated polydimethylsiloxane, cocamidomethyl MEA, polyquaternium salt, lactobacillus fermentation lysate, white truffle extract, and dipotassium glycyrrhizate to prepare a composition with significant color-fixing effect through the synergistic action of each component. This composition can be used in shampoos and conditioners with color-fixing properties. Attached Figure Description

[0026] Other features, objects, and advantages of the present invention will become more apparent from the following detailed description of non-limiting embodiments with reference to the accompanying drawings:

[0027] Figure 1 These are photographs of hair strands before and after treatment using the test products of Example 1 and the negative control. Detailed Implementation

[0028] The present invention will now be described in detail with reference to specific embodiments. These embodiments will help those skilled in the art to further understand the present invention, but do not limit the invention in any way. It should be noted that those skilled in the art can make various modifications and improvements without departing from the concept of the present invention. These all fall within the scope of protection of the present invention.

[0029] The terms "preferred," "more preferably," and "more suitable" used in this invention refer to embodiments of the invention that provide certain beneficial effects under certain circumstances. However, other embodiments may also be preferred under the same or other circumstances. Furthermore, the description of one or more preferred embodiments does not imply that other embodiments are unavailable, nor is it intended to exclude other embodiments from the scope of this invention.

[0030] It should be understood that, except in any operational instance or otherwise indicated, all figures representing the amounts of ingredients used, for example, in the specification and claims, should be understood to be modified in all cases by the term "about". Therefore, unless otherwise stated, the numerical parameters set forth in the following specification and appended claims are approximations varying with the desired performance to be obtained according to the invention. It is not at all an attempt to limit the application of the doctrine of equivalents to the scope of the claims; each numerical parameter should be interpreted at least according to the number of significant figures reported and by applying ordinary rounding techniques.

[0031] Although the numerical ranges and parameters illustrating the broad scope of the invention are approximate, the values ​​listed in the specific examples are reported as precisely as possible. However, any numerical value inherently contains some error that is necessarily caused by the standard deviation found in their respective test measurements.

[0032] The following embodiments provide a color-fixing hair composition comprising the following components: amino-terminated polydimethylsiloxane, polyquaternium salt, cocamidomethyl MEA, lactobacillus fermentation lysate, white truffle extract, hydroxyethyl urea, and dipotassium glycyrrhizate.

[0033] In one specific embodiment, the amino-terminated polydimethylsiloxane is derived from commercial products. ADM 8600E is composed of: water, ammonia-terminated polydimethylsiloxane, tridecyl alcohol polyether-5, glycerol, tridecyl alcohol polyether-10, polydimethylsiloxane, trimethylsiloxysilicate, phenoxyethanol, and acetic acid (i.e., the following: water / ammonia-terminated polydimethylsiloxane / tridecyl alcohol polyether-5 / glycerol / tridecyl alcohol polyether-10 / polydimethylsiloxane / trimethylsiloxysilicate / phenoxyethanol / acetic acid). The ammonia-terminated polydimethylsiloxane used in this invention can also be provided by other commercially available raw materials; this invention does not impose any particular limitation.

[0034] In one specific embodiment, the cocamide methyl MEA / glycerin is derived from the commercial MICONOL CMM. The cocamide methyl MEA may also be provided by other commercial raw materials, and the present invention does not impose any particular limitation.

[0035] In one specific embodiment, the polyquaternium-7 is derived from the commercial product ME POLYMER 09WPF(C), and its components are: water, polyquaternium-7, and sodium benzoate (i.e., the following water / polyquaternium-7 / sodium benzoate). The polyquaternium-7 used in this invention can also be provided by other commercial raw materials, and this invention does not impose any particular limitation.

[0036] In one specific embodiment, the polyquaternium-10 is derived from the commercial product CATINAI HC-200. Its components are: polyquaternium-10, sodium chloride, and water (i.e., polyquaternium-10 / sodium chloride / water as described below). The polyquaternium-10 used in this invention can also be provided by other commercial raw materials; this invention does not impose any particular limitation.

[0037] In one specific embodiment, the Lactobacillus fermentation lysate and the Tuber Magnatum extract are derived from the commercial product Fermented Truffle Mushroom Liquid Extract V2 (manufactured by Draco Natural Products Inc.), whose components are: Lactobacillus fermentation lysate, Tuber Magnatum extract, capryloyl hydroxamic acid, caprylyl glycol, and glycerin (i.e., the following Lactobacillus fermentation lysate / Tuber Magnatum extract / capryloyl hydroxamic acid / caprylyl glycol / glycerin). The Lactobacillus fermentation lysate contains various substances that promote skin metabolism, effectively improving the respiration capacity of skin cells, making cells more vibrant, enhancing the synthesis of adenosine triphosphate (ATP), increasing cellular energy, promoting the synthesis of collagen and hyaluronic acid, and promoting skin renewal, reducing melanin synthesis, and scavenging free radicals. White truffle (TUBER MAGNATUM) extract is an active ingredient extracted from Italian white truffle (Latin name: T. magnatum Vittad). It is rich in over 50 active ingredients, including 17 amino acids (including the 8 essential amino acids that the human body cannot synthesize), 8 vitamins, proteins, various unsaturated fatty acids, essential trace elements such as zinc, manganese, iron, phosphorus, and selenium, as well as a large number of metabolites such as androsterone, sphingolipids, truffle acid, sterols, truffle polysaccharides and polypeptides, fatty acids, and trace elements. It can effectively decompose and metabolize melanin, thereby inhibiting melanin production and achieving a whitening effect. The lactobacillus fermentation lysate and white truffle extract used in this invention can also be provided by other commercial raw materials; this invention does not impose any particular limitations.

[0038] In one specific embodiment, the hair-fixing composition comprises the following components in parts by weight: 1-5 parts of water / ammonia-terminated polydimethylsiloxane / tridecyl alcohol polyether-5 / glycerin / tridecyl alcohol polyether-10 / polydimethylsiloxane / trimethylsiloxysilicate / phenoxyethanol / acetic acid, 0.5-2.5 parts of cocamidomethyl MEA / glycerin, 1-2 parts of water / polyquaternium-7 / sodium benzoate, 0.4-0.8 parts of polyquaternium-10 / sodium chloride / water, 0.3-0.5 parts of water / hydroxyethyl urea, 0.1-0.5 parts of lactobacillus fermentation lysate / white truffle extract / capryloyl hydroxamic acid / caprylyl glycol / glycerin, and 0.01-0.05 parts of dipotassium glycyrrhizate.

[0039] The aforementioned color-fixing hair composition can be used to prepare shampoo and conditioner products of any dosage form.

[0040] The following embodiments also specifically provide a color-fixing shampoo, comprising the following components in parts by weight: water / ammonia-terminated polydimethylsiloxane / tridecyl alcohol polyether-5 / glycerin / tridecyl alcohol polyether-10 / polydimethylsiloxane / trimethylsiloxysilicate / phenoxyethanol / acetic acid 1-5 parts, cocamidomethyl MEA / glycerin 0.5-2.5 parts, water / polyquaternium-7 / sodium benzoate 1-2 parts, polyquaternium-10 / sodium chloride / water 0. 4-0.8 parts, water / hydroxyethyl urea 0.3-0.5 parts, Lactobacillus fermentation lysate / white truffle extract / capryloyl hydroxamic acid / caprylyl glycol / glycerin 0.1-0.5 parts, dipotassium glycyrrhizate 0.01-0.05 parts, surfactant 10-20 parts, pH adjuster 0.1-0.5 parts, humectant 0.1-0.2 parts, fragrance 0-0.5 parts, preservative 0-1 part, chelating agent 0-0.1 parts, solvent to make up to 100 parts.

[0041] In one specific embodiment, the solvent is water;

[0042] The surfactant is selected from sodium lauryl ether sulfate, cocamidopropyl betaine, and sodium cocoyl methyl taurate taurate; for example, sodium lauryl ether sulfate is derived from raw materials. N 70 contains sodium lauryl ether sulfate and water (i.e., sodium lauryl ether sulfate / water as described below, with a sodium lauryl ether sulfate content of 70%); cocamidopropyl betaine is derived from the raw material. Betain F 50 contains cocamidopropyl betaine, water, and citric acid (i.e., the following cocamidopropyl betaine / water / citric acid, with cocamidopropyl betaine content of 44.2%); sodium cocoyl methyl taurate is derived from raw material NEOSCOAP CDT-30-SF, containing sodium cocoyl methyl taurate / water / sodium chloride (i.e., the following sodium cocoyl methyl taurate / water / sodium chloride, with sodium cocoyl methyl taurate content of 26%).

[0043] The pH adjuster is selected from citric acid;

[0044] The humectant is selected from panthenol;

[0045] The fragrance agent is selected from flavorings;

[0046] The preservative is selected from phenoxyethanol and sodium benzoate;

[0047] The chelating agent is selected from disodium EDTA.

[0048] In the following examples, all other raw materials used are commercially available.

[0049] Example 1

[0050] This embodiment provides a color-fixing shampoo, the composition and weight ratio of its raw materials (total weight parts of 100) are shown in Table 1. The specific steps of the preparation method of the shampoo are as follows:

[0051] 1. Clean and disinfect the mixing pot before manufacturing.

[0052] 2. Add water and sodium lauryl ether sulfate / water to a pot, heat to 80-85℃ and stir to dissolve evenly. Then add polyquaternium-10 / sodium chloride / water and homogenize until the raw materials are completely dissolved.

[0053] 3. Maintain the temperature at 80-85℃, add cocamidopropyl betaine / water / citric acid, sodium cocoyl methyl taurate / water / sodium chloride, water / polyquaternium-7 / sodium benzoate, cocamidomethyl MEA / glycerol, disodium EDTA, and stir until the raw materials are completely dissolved and homogeneous;

[0054] 4. Once the temperature drops to 65℃, add phenoxyethanol and sodium benzoate, and stir thoroughly until dissolved and homogeneous;

[0055] 5. Once the temperature drops to 45℃, add the raw materials: water / ammonia-terminated polydimethylsiloxane / tetranol polyether-5 / glycerin / tetranol polyether-10 / polydimethylsiloxane / trimethylsiloxane / phenoxyethanol / acetic acid, (daily use) fragrance, water / hydroxyethyl urea, lactobacillus fermentation lysate / white truffle (TUBER MAGNATUM) extract / capryloyl hydroxamic acid / caprylyl glycol / glycerin, citric acid, panthenol, and dipotassium glycyrrhizate. Stir thoroughly and dissolve evenly.

[0056] 6. Filter the material to obtain the color-fixing shampoo.

[0057] Example 2

[0058] This embodiment provides a color-fixing shampoo, the composition and weight ratio of its raw materials (total weight parts of 100) are shown in Table 1. The preparation steps of the shampoo are the same as in Embodiment 1.

[0059] Example 3

[0060] This embodiment provides a color-fixing shampoo, the composition and weight ratio of its raw materials (total weight parts of 100) are shown in Table 1. The preparation steps of the shampoo are the same as in Embodiment 1.

[0061] Example 4

[0062] This embodiment provides a color-fixing shampoo, the composition and weight ratio of its raw materials (total weight parts of 100) are shown in Table 1. The preparation steps of the shampoo are the same as in Embodiment 1.

[0063] Example 5

[0064] This embodiment provides a color-fixing shampoo, the composition and weight ratio of its raw materials (total weight parts of 100) are shown in Table 1. The preparation steps of the shampoo are the same as in Embodiment 1.

[0065] Table 1

[0066]

[0067]

[0068] Comparative Example 1

[0069] This comparative example provides a color-fixing shampoo, the composition and weight ratio of its raw materials (total weight parts of 100) are shown in Table 2. Compared with Example 2, the weight parts of water / ammonia-terminated polydimethylsiloxane / tridecyl alcohol polyether-5 / glycerin / tridecyl alcohol polyether-10 / polydimethylsiloxane / trimethylsiloxysilicate / phenoxyethanol / acetic acid are 1.5 parts, and no cocamide methyl MEA / glycerin is added. The preparation steps of the shampoo are the same as those in Example 2.

[0070] Comparative Example 2

[0071] This comparative example provides a color-fixing shampoo, the composition and weight ratio of its raw materials (total weight parts of 100) are shown in Table 2. Compared with Example 2, it does not contain Lactobacillus fermentation lysate / Tubermaganum extract / capryloyl hydroxamic acid / caprylyl glycol / glycerin. The preparation steps of the shampoo are the same as those in Example 2.

[0072] Comparative Example 3

[0073] This comparative example provides a color-fixing shampoo, the composition and weight ratio of its raw materials (total weight parts of 100 parts) are shown in Table 2. Compared with Example 2, the weight parts of Lactobacillus fermentation lysate / TUBERMAGNATUM extract / capryloyl hydroxamic acid / caprylyl glycol / glycerin used are 0.05 parts. The preparation steps of the shampoo are the same as those in Example 2.

[0074] Comparative Example 4

[0075] This comparative example provides a color-fixing shampoo, the composition and weight ratio of its raw materials (total weight parts of 100) are shown in Table 2. Compared with Example 2, lactic acid bacteria fermentation lysate / sodium chloride / sodium benzoate is used instead of lactic acid bacteria fermentation lysate / Tuber Magnatum extract / caprylyl hydroxamic acid / caprylyl glycol / glycerin. The preparation steps of the shampoo are the same as those in Example 2.

[0076] Comparative Example 5

[0077] This comparative example provides a color-fixing shampoo, the composition and weight ratio of its raw materials (total weight parts of 100) are shown in Table 2. Compared with Example 2, water / hydroxyethyl urea is not added. The preparation steps of the shampoo are the same as those of Example 2.

[0078] Comparative Example 6

[0079] This comparative example provides a color-fixing shampoo, the composition and weight ratio of its raw materials (total weight parts of 100) are shown in Table 2. Compared with Example 2, the weight parts of water / polyquaternium-7 / sodium benzoate are 2.5 parts, and the weight parts of polyquaternium-10 / sodium chloride / water are 0.3 parts. The preparation steps of the shampoo are the same as those in Example 2.

[0080] Comparative Example 7

[0081] This comparative example provides a color-fixing shampoo, the composition and weight ratio of its raw materials (total weight parts of 100) are shown in Table 2. Compared with Example 3, the weight parts of water / polyquaternium-7 / sodium benzoate are 0.8 parts, and the weight parts of polyquaternium-10 / sodium chloride / water are 0.8 parts. The preparation steps of the shampoo are the same as those in Example 3.

[0082] Table 2

[0083]

[0084]

[0085] Efficacy verification:

[0086] The shampoos prepared in Examples 1-5 and Comparative Examples 1-7 were used as test samples, and a 10 g / L sodium dodecyl sulfate solution was used as a negative control sample. The hair color care efficacy of the test products was evaluated through subjective assessment, image analysis, and instrumental testing. The specific test method used is from PONY-SOPR-24514.01 "Test Method for Hair Color Care Efficacy of Shampoo and Conditioner Products".

[0087] 1) Test hair strand: 15cm*1.5cm*2g of detached damaged yellow hair strand.

[0088] 2) Testing instruments and reagents

[0089] 2.1 Colorimeter probe, color difference testing instrument

[0090] 2.2 VISIA-CR Facial Image Analyzer

[0091] 2.3 Electric thermostatic water bath: Temperature range includes 40.0℃ ± 1.0℃

[0092] 2.4 Electronic Balance

[0093] 2.5 10 g / L sodium dodecyl sulfate solution

[0094] 2.6 Comb

[0095] 3) Testing Environment

[0096] The test environment temperature was 20.0℃~22.0℃ and the ambient humidity was 40.0%~60.0%, which met the requirements of the design scheme.

[0097] 4) Test Indicators

[0098] 4.1 Subjective Evaluation

[0099] Researchers visually observed hair strands and subjectively scored the differences in color. The assessment criteria were as follows: "0" represented no significant color change; "1" represented slight fading; "2" represented significant fading; and "3" represented severe fading.

[0100] 4.2 Efficacy Testing

[0101] Color intensity parameter analysis: IPP software is used to analyze photos of hair strands before and after product use. By comparing the number of pixels in a certain gray range, the more pixels there are, the darker the color of the hair strand.

[0102] Color difference parameter △E analysis: △E=SQRT(△L*2+△a*2+△b*2), the smaller the △E value, the less the color change of the hair strand.

[0103] 5) Testing methods

[0104] 5.1 Soak the selected hair strands in a 10g / L sodium dodecyl sulfate solution, bathe in a 40℃ constant temperature water bath for 30 minutes, and then rinse thoroughly with clean water. Next, gently comb the wet hair strands 10 times and hang them in a constant temperature and humidity environment for 8–24 hours.

[0105] 5.2 Re-weigh the hair bundle and select the hair bundle with a weight deviation of ±0.2g for the next step;

[0106] 5.3 Randomly group the selected hair strands into groups of 5 strands each;

[0107] 5.4 Comb the hair strands repeatedly 10 times to separate each strand and remove any knots;

[0108] 5.5 After smoothing and fixing the hair strand surface, use the Colorimeter probe to measure the test sample group, negative control group, and positive control group, and record the basic L* value, a* value, and b* value of the hair strand surface before sampling; use the VISIA-CR facial image analyzer to take pictures of the test sample group, negative control group, and positive control group respectively, and use software to analyze the basic color intensity value of the hair strand as the initial test value.

[0109] 5.6 Apply 0.2 mL / g of hair to each group of hair bundles for 1 min, then rinse with water for 30 s. Every 5 s, squeeze the water off the hair from top to bottom, and repeat the above shampooing process once. After the shampooing process, gently comb the wet hair bundles 10 times with a comb, and hang the hair bundles in an environment with a temperature of 21±1℃ and a relative humidity of 50±10%RH for 8 to 24 hours.

[0110] 5.7 Repeat the shampooing process in step 5.6 once a day; collect data after 14 days and 28 days: After combing and fixing the hair strands, use the Colorimeter probe to measure the test sample group, negative control group and positive control group, record the L* value, a* value and b* value of the hair strand surface, and calculate the color difference parameter ΔE value; take pictures of the test sample group, negative control group and positive control group with the VISIA-CR facial image analyzer, and analyze the color intensity value of the hair strands with software.

[0111] Researchers visually observed each group of hair strands, subjectively judged whether the hair strand color changed, and scored the results.

[0112] 6) Test Results

[0113] 6.1 The scores of the subjective assessment results conducted by the researchers 14 days (D14) and 28 days (D28) after shampooing of each group of hair strands are shown in Table 3.

[0114] Table 3

[0115]

[0116]

[0117] 6.2 Based on the initial color intensity parameter value of each test sample group's hair strand, and the color intensity parameter value after 14 days (D14) and 28 days (D28) of shampooing, the color intensity parameter change rate compared to the initial color intensity parameter was obtained (color intensity parameter change rate = (color intensity parameter value after shampooing - initial color intensity parameter value) / initial color intensity parameter value * 100%), and the results are shown in Table 4.

[0118] Table 4

[0119]

[0120] 6.3 Based on the L*, a*, and b* values ​​of each test sample group after 14 days (D14) and 28 days (D28) of hair washing, the color difference parameter △E value after washing was calculated, and the results are shown in Table 5.

[0121] Table 5

[0122]

[0123] As can be seen from the results in Tables 3-5, the subjective scores, color intensity parameters, and color difference parameter ΔE values ​​of the shampoos prepared in each embodiment as test samples were significantly improved compared with the negative control samples, indicating that the shampoos prepared in this invention have a significant color-fixing effect.

[0124] Furthermore, a comparison of the effects of Example 2 and Comparative Examples 1-6 shows that when the color-fixing hair-setting composition does not contain cocamide methyl MEA / glycerin, does not contain Lactobacillus fermentation lysate / Tuber Magnatum extract / capryloyl hydroxamic acid / caprylyl glycol / glycerin, when the content of added Lactobacillus fermentation lysate / Tuber Magnatum extract / capryloyl hydroxamic acid / caprylyl glycol / glycerin is too low, when Lactobacillus fermentation lysate / sodium chloride / sodium benzoate is used instead of Lactobacillus fermentation lysate / Tuber Magnatum extract / capryloyl hydroxamic acid / caprylyl glycol / glycerin, when water / hydroxyethyl urea is not added, and when the content of water / polyquaternium-7 / sodium benzoate is too high, the color intensity parameter change rate and color difference parameter ΔE value all show varying degrees of increase compared to Example 2. As can be seen from the comparison of the effects of Example 3 and Comparative Example 7, when the content of water / polyquaternium-7 / sodium benzoate in the composition of the color-fixing hair product is too low, the change rate of color intensity parameter and the color difference parameter ΔE value also increase compared with Example 3.

[0125] Furthermore, a comparison of Examples 1 and 4-5 shows that when the ratio of water / ammonia-terminated polydimethylsiloxane / trigetromethorphan-5 / glycerol / trigetromethorphan-10 / polydimethylsiloxane / trimethylsiloxysilicate / phenoxyethanol / acetic acid and cocamidomethylMEA / glycerol is 2:1, the color intensity parameter change rate after 14 days and 28 days is only -0.46% and -0.71%, and the color difference parameter ΔE value is only 0.83 and 1.20; while when the ratio is not this, both the color intensity parameter change rate and the color difference parameter ΔE value increase. This indicates that by specifically selecting the ratio of these two components, the color fixing effect can be further improved.

[0126] Figure 1 The following is an effective example of treating hair strands before and after treatment using test samples from Example 1 and the negative control. As can be seen from the comparison, the hair strands of the negative control showed a significant color change before and after treatment, while the hair strands of Example 1 did not show a significant color change before and after treatment.

[0127] This invention has many specific applications, and the above description is only a preferred embodiment. It should be noted that the above embodiments are for illustrative purposes only and are not intended to limit the scope of protection of this invention. For those skilled in the art, several improvements can be made without departing from the principle of this invention, and these improvements should also be considered within the scope of protection of this invention.

Claims

1. A color-fixing hair composition, characterized in that, The hair color fixing composition comprises the following components in parts by weight: 1-5 parts of water / ammonia-terminated polydimethylsiloxane / tridecyl alcohol polyether-5 / glycerin / tridecyl alcohol polyether-10 / polydimethylsiloxane / trimethylsiloxane / phenoxyethanol / acetic acid, 0.5-2.5 parts of cocamidomethyl MEA / glycerin, 1-2 parts of water / polyquaternium-7 / sodium benzoate, 0.4-0.8 parts of polyquaternium-10 / sodium chloride / water, 0.3-0.5 parts of water / hydroxyethyl urea, 0.1-0.5 parts of lactobacillus fermentation lysate / white truffle extract / capryloyl hydroxamic acid / caprylyl glycol / glycerin, and 0.01-0.05 parts of dipotassium glycyrrhizate; The commercial name of the water / ammonia-terminated polydimethylsiloxane / tridecyl alcohol polyether-5 / glycerol / tridecyl alcohol polyether-10 / polydimethylsiloxane / trimethylsiloxysilicate / phenoxyethanol / acetic acid is BELSIL® ADM 8600 E; The commercial name of the cocamide methyl MEA / glycerin is MICONOL CMM; The commercial name of the water / polyquaternium-7 / sodium benzoate is ME POLYMER 09WPF(C); The product name of the water / hydroxyethyl urea is HYDROVANCE XTEND; The trade name of the fermentation lysate of *Acidobacterium* / *White Truffle* extract / *Capryloyl Hydroxamic Acid* / *Caprylyl Glycol* / *Glycerin* is Fermented Truffle Mushroom Liquid Extract V2.

2. The hair-fixing composition according to claim 1, characterized in that, The weight ratio of water / ammonia-terminated polydimethylsiloxane / tetranol polyether-5 / glycerol / tetranol polyether-10 / polydimethylsiloxane / trimethylsiloxysilicate / phenoxyethanol / acetic acid to cocamidomethylMEA / glycerol is 2:

1.

3. The use of a color-fixing hair composition according to any one of claims 1-2 in the preparation of shampoo and hair care products.

4. The application according to claim 3, characterized in that, The hair care products include shampoo, conditioner, and hair mask.

5. A color-fixing shampoo, characterized in that, The hair color fixing composition according to any one of claims 1-2 further includes at least one of a solvent, surfactant, pH adjuster, humectant, fragrance, preservative, and chelating agent.

6. The color-fixing shampoo according to claim 5, characterized in that, The solvent is water; The surfactant is selected from sodium laureth sulfate, cocamidopropyl betaine, and sodium cocoyl methyl taurate taurate. The pH adjuster is selected from citric acid; The humectant is selected from panthenol; The fragrance agent is selected from flavorings; The preservative is selected from phenoxyethanol and sodium benzoate; The chelating agent is selected from disodium EDTA.

7. The color-fixing shampoo according to claim 6, characterized in that, The components include the following parts by weight: 1-5 parts of water / ammonia-terminated polydimethylsiloxane / tridecyl alcohol polyether-5 / glycerin / tridecyl alcohol polyether-10 / polydimethylsiloxane / trimethylsiloxysilicate / phenoxyethanol / acetic acid, 0.5-2.5 parts of cocamidomethyl MEA / glycerin, 1-2 parts of water / polyquaternium-7 / sodium benzoate, 0.4-0.8 parts of polyquaternium-10 / sodium chloride / water, 0.3-0.5 parts of water / hydroxyethyl urea, 0.1-0.5 parts of lactobacillus fermentation lysate / white truffle extract / capryloyl hydroxamic acid / caprylyl glycol / glycerin, 0.01-0.05 parts of dipotassium glycyrrhizate, 10-20 parts of surfactant, 0.1-0.5 parts of pH adjuster, 0.1-0.2 parts of humectant, 0-0.5 parts of fragrance, 0-1 part of preservative, 0-0.1 parts of chelating agent, and solvent to bring the total to 100 parts.

8. A method for preparing a color-fixing shampoo according to any one of claims 5-7, characterized in that, Includes the following steps: Weigh out each component of the color-fixing hair composition according to any one of claims 1-2, as well as the moisturizer, emollient, thickener, chelating agent, fragrance and preservative in proportion, add them to the solvent, and stir evenly to obtain the color-fixing shampoo.

Images