一种交联型聚丙烯酰胺生产工艺

By spraying a hydrophobic nano-ceramic coating onto the inner wall of the polymerization reactor and controlling the reaction temperature, combined with a four-roll mill and a dual-chamber high-square sieve, the problem of colloid residue on the reactor wall was solved, improving production efficiency and product yield while reducing costs.

CN117285677BActive Publication Date: 2026-07-17PETROCHINA CO LTD

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
PETROCHINA CO LTD
Filing Date
2022-06-17
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

In the existing polyacrylamide powder production process, the colloid generated after the polymerization reaction remains on the reactor wall, resulting in severe glue adhesion, which affects the continuity of production. In addition, the grinding and screening efficiency is low, leading to low production capacity and product yield.

Method used

The inner wall of the polymerization reactor is polished and coated with a hydrophobic nano-ceramic coating made of stainless steel. The polymerization reaction temperature is controlled and the reactor is vented at high temperature. The colloid is then ground and screened using a four-roll mill and a double-chamber high square screen to control the particle size.

Benefits of technology

It effectively prevents colloids from remaining on the reactor wall, improves the production line's processing capacity and product yield, and reduces production costs.

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Abstract

本发明涉及一种交联型聚丙烯酰胺生产工艺。主要解决了现有聚合反应后生成的胶体在反应器器壁残留形成严重挂胶及研磨、筛分效率低而不能进行连续稳定生产的问题。该方法包括:1)、原料溶解配置反应液;2)、聚合反应:将反应液转移到聚合反应器中,向反应器中加入二段引发剂,吹入氮气除氧后向反应器中依次加入一段引发剂,引发聚合反应,升温后停吹入氮气,控制反应压力;反应结束后将反应器中生成的胶体压出聚合反应器;3)、对聚合后的胶体进行造粒、干燥、研磨、筛分处理:获得粒径在0.30~0.15mm的交联型聚丙烯酰胺粉剂产品。该生产工艺,能够防止聚合生成的胶体在反应器器壁残留,物料的筛分效率高。
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