一种六氟磷酸锂反应装置及工艺
By designing a degassing and ripening unit and a multi-stage stirring reaction unit in the lithium hexafluorophosphate reactor, and utilizing a disc turbine propeller to shear the gas phase, the problems of low gas-liquid contact efficiency and high equipment complexity in the existing technology are solved, achieving efficient gas-liquid contact and a simplified operation process.
Patent Information
- Authority / Receiving Office
- CN · China
- Patent Type
- Patents(China)
- Current Assignee / Owner
- ZHEJIANG INST OF TIANJIN UNIV (SHAOXING)
- Filing Date
- 2023-10-10
- Publication Date
- 2026-07-17
AI Technical Summary
The existing lithium hexafluorophosphate production process has problems such as a large number of equipment, low reactor utilization, complex pipeline connections, and high difficulty in equipment operation and maintenance. In particular, the gas-liquid contact efficiency is low and bubble aggregation is easy to occur in multi-stage series reactors.
A lithium hexafluorophosphate reactor is used, which includes a reactor body, a degassing and ripening unit and multiple stirring reaction units. Each stirring reaction unit is equipped with a multi-stage stirrer and a gas distributor, which are connected by stage partitions and gas lift channels. The gas phase is sheared by straight or oblique blade disk turbines to ensure gas-liquid countercurrent contact, and the gas-liquid contact efficiency is improved by controlling the gas distribution and stirring speed.
This technology enables multi-stage countercurrent gas-liquid contact within a single reactor, improving gas-liquid contact efficiency, reducing system complexity and operational difficulty, enhancing reactor utilization, and preventing a decrease in contact efficiency caused by bubble coalescence.
Smart Images
Figure CN117299047B_ABST