石墨烯薄膜的制备方法及系统

Electrolysis of graphene oxide films via electrochemical reduction solves the problems of long production cycles and high costs associated with graphene films, enabling efficient and low-energy-consumption preparation of graphene films, which is suitable for large-scale production.

CN117342548BActive Publication Date: 2026-07-17THE SIXTH ELEMENT CHANGZHOU MATERIALS TECH

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
THE SIXTH ELEMENT CHANGZHOU MATERIALS TECH
Filing Date
2022-06-29
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Existing methods for preparing graphene films suffer from long production cycles, high costs, and low efficiency. In particular, the traditional thermal reduction method is energy-intensive and requires stringent conditions, which hinders its large-scale production.

Method used

An electrochemical reduction method is employed, in which graphene oxide films are electrolyzed in an electrolyte solution. By selecting appropriate electrolysis modes and parameters, including constant voltage or constant current modes, and combining them with a three-electrode system, efficient reduction of graphene oxide can be achieved.

Benefits of technology

It shortens the preparation time of graphene films, improves reduction efficiency, reduces production costs, reduces energy consumption, and enhances the quality and production efficiency of graphene films.

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Abstract

本发明提供一种石墨烯薄膜的制备方法及系统,包括:制备氧化石墨烯薄膜;将氧化石墨烯薄膜置于电解质溶液中,根据氧化石墨烯薄膜的厚度选择电解模式并进行电解;根据电解时间达到电解预设时间,停止电解,石墨烯薄膜制备完成。本制备方法,本发明在石墨烯薄膜的生产工艺中引入电化学还原方法,由原始的“热还原”转变成“电化学还原”,本发明提供的制备方法与传统的热还原相比,设备简单,可调控性强,操作简单易上手,且能耗小,有利于实现“双碳”目标。通过改变氧化石墨烯的生产工艺,将电化学引入其中,不仅可以有效地缩短石墨烯薄膜的制备时间,大大提高了还原效率,提升了能源的利用率,而且还能降低石墨烯的生产成本。
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