一种双圆台衬底托辅助异质外延大尺寸单晶金刚石的方法

CN117431622BActive Publication Date: 2026-07-17JILIN UNIVERSITY +1

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
JILIN UNIVERSITY
Filing Date
2023-10-27
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

When preparing large-size single-crystal diamonds using heteroepitaxial growth, the uneven temperature distribution on the sample surface leads to poor diamond growth quality and potential sample breakage.

Method used

A dual-frustum substrate-assisted heteroepitaxial method is designed. The electric field distribution inside the cavity is simulated using Comsol software, the structural parameters of the substrate holder are optimized, the electric field uniformity on the sample stage surface is ensured, thereby improving temperature uniformity and ultimately obtaining high-quality single-crystal diamond.

Benefits of technology

This method achieves a uniform distribution of electric field and temperature on the sample stage surface, improves the electric field strength of the cavity, optimizes the diamond growth temperature, and obtains high-quality, large-size single-crystal diamonds.

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Abstract

本发明公开了一种双圆台衬底托辅助异质外延大尺寸单晶金刚石的方法,属于微波等离子体化学气相沉积技术领域,使用Comsol软件模拟不同尺寸衬底圆台观测腔体内电场强度分布情况,通过仿真得到合适的样品台尺寸,建立双圆台实物,随后采用双圆台结构在CVD设备上的Ir / SrTiO3复合衬底表面进行金刚石的偏压增强成核与生长,最终获得大尺寸的单晶金刚石。通过设计的双圆台衬底托,使得腔体内的次生电场的数值相对于原始样品台变得更小,样品台的电场分布更加均匀,对于腔体的等离子体的分布产生更小的影响,利于等离子体的分布汇聚,更适合金刚石的高质量生长,为进一步实现大尺寸单晶金刚石制备提供基础。
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