一种高纯度木犀草苷的提取分离方法
By combining Soxhlet extraction and silica gel column separation with methanol crystallization, high-purity luteolin glycosides can be efficiently extracted from chrysanthemum, solving the problems of poor extraction effect and high cost in existing technologies, and realizing high-purity and low-cost industrial production.
Patent Information
- Authority / Receiving Office
- CN · China
- Patent Type
- Patents(China)
- Current Assignee / Owner
- HUBEI MINGMU HEALTH TECH CO LTD
- Filing Date
- 2023-11-03
- Publication Date
- 2026-07-17
AI Technical Summary
Existing technologies are difficult to efficiently extract high-purity luteolin from chrysanthemums, and the cost is high, especially since column chromatography separation is not very effective.
A method combining Soxhlet extraction and vacuum concentration with silica gel column separation, including primary and secondary medium-pressure separation, combined with methanol crystallization, was adopted to achieve efficient separation of luteolin by controlling parameters such as the particle size of dried chrysanthemum powder, the ratio of extractant, the particle size of silica gel powder, and the pressure.
The extraction of high-purity luteolin glycosides has been achieved, with a purity of over 96%. The raw materials are widely available, low in cost, and suitable for industrial production.
Smart Images
Figure CN117486957B_ABST