一种难熔高熵合金块体及制备方法

By employing a sintering method combining high current density pulsed current and high pressure with an ultra-fast heating rate, the problems of long preparation time and low density of refractory high-entropy alloy bulk materials have been solved, achieving efficient and low-cost preparation of refractory high-entropy alloy bulk materials with high metallurgical bonding strength and excellent corrosion resistance.

CN117531997BActive Publication Date: 2026-07-17UNIV OF SCI & TECH BEIJING

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
UNIV OF SCI & TECH BEIJING
Filing Date
2023-11-09
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Existing technologies are insufficient to prepare refractory high-entropy alloy bulk materials with high density and high microstructure uniformity in a short period of time, and also suffer from high production costs and low efficiency.

Method used

A method combining high current density pulsed current and high pressure with an ultra-fast heating rate was used to rapidly sinter refractory high entropy alloy powder in a sintering device. A sintering mold composed of graphite foil and insulating corundum tube was used to improve temperature uniformity and prevent contamination, thus producing a high-density refractory high entropy alloy bulk.

Benefits of technology

High density and uniform microstructure of refractory high-entropy alloy blocks were achieved in a short time, improving the metallurgical bonding strength, corrosion resistance and oxidation resistance of the material, and reducing production time and energy consumption.

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Abstract

本发明涉及一种难熔高熵合金块体及制备方法,方法包括:将待烧结的难熔高熵合金粉末原料放置在烧结装置中;对所述烧结装置施加一定的压力和设定参数的脉冲电流,经过设定的时间后,得到难熔高熵合金块体,所述设定参数包括:电压500~3500V / m,电流密度为3.0~9.0×106A / m2、频率1~100kHz,脉冲宽度为1.0~10.0μs。本发明可对熔点极高、难以均匀致密的难熔高熵合金粉末进行烧结,可实现在短时间内制备出组织均匀、致密度超过98%的难熔高熵合金块体。
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