一种通过超声波提纯5mm以下等外海绵钛的方法

By using ultrasonic separation technology under inert gas protection to smelt sponge titanium, the problem of low purification efficiency of non-grade sponge titanium has been solved, and efficient purification and high-purity product production have been achieved.

CN117568626BActive Publication Date: 2026-07-17CHAOYANG JINDA TITANIUM IND CO LTD

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
CHAOYANG JINDA TITANIUM IND CO LTD
Filing Date
2023-11-20
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Existing technologies are insufficient for efficiently purifying out-of-grade titanium sponges smaller than 5mm, which significantly reduces their value in the titanium industry and fails to meet the requirements for large-scale production.

Method used

Ultrasonic separation technology is used to melt sponge titanium under inert gas protection. An ultrasonic generator is used to apply ultrasonic action at the solid-liquid interface. Combined with a vacuum environment, temperature and pulling speed are controlled to achieve rapid diffusion and uniform distribution of impurity elements.

Benefits of technology

It significantly improves the purification efficiency of impurity elements, enhances product quality and purity, reduces the entry of oxygen and hydrogen atoms, and ensures the high purity and stability of the product.

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Abstract

本发明涉及一种通过超声波提纯5mm以下等外海绵钛的方法,包括步骤有:选出颗粒小于5mm的等外海绵钛;反应器抽真空充氩气通电升温加热;安装超声发射器并开启,频率设定为0.5kW‑12kW;控制结晶速度,缓慢向上提拉发射器,提拉速度和结晶速度保持相同。本方法在保护性气体氩气保护下的熔炼和超声提纯,降低提纯过程中氧原子和氢原子的进入;通过超声发射器直接对固液界面施加超声作用,使排除的杂质在熔体中迅速扩散,其气穴效应产生高速液流搅拌,使熔体中的杂质元素分布均匀一致,可以有效避免提纯后产品中杂质元素的元元素偏析。
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