一种废旧石英坩埚的高效回收方法

By separating and purifying waste quartz crucibles using laser irradiation and wet acid leaching technology, the problem of recycling waste quartz crucibles has been solved, enabling the production of high-efficiency, high-purity recycled quartz powder, which is suitable for the comprehensive recycling and utilization of photovoltaic solid waste resources.

CN117800589BActive Publication Date: 2026-07-17KUNMING UNIV OF SCI & TECH

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
KUNMING UNIV OF SCI & TECH
Filing Date
2024-01-10
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Waste quartz crucibles are difficult to recycle efficiently, mainly because the inner and outer walls contain quartz layers and the middle layer of quartz glass, which are difficult to separate. In addition, the crucibles are heavily contaminated with impurities, resulting in low recycling efficiency and low product purity, making them unsuitable for use as high-value products.

Method used

Laser irradiation is used to separate the cristobalite layer on the surface of waste quartz crucibles. Combined with wet acid leaching technology, the impurities are diffused to the surface of the amorphous silica layer by the heating effect of laser irradiation. The impurities are then removed by acid washing, achieving efficient separation and purification.

Benefits of technology

This method improves the purity and recycling efficiency of quartz glass, yields high-purity recycled quartz powder products, is highly adaptable, and is easy to scale up for production, thus achieving efficient recycling and high-value utilization of waste quartz crucibles.

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Abstract

本发明涉及一种废旧石英坩埚的高效回收方法,属于光伏固废资源综合回收与利用技术领域。本发明将废旧石英坩埚破碎,根据粒度进行分级得到不同粒度级别的废旧石英块体;分别将不同粒度级别的废旧石英块体加入到着色液中进行着色处理,然后分别进行激光照射实现分离焙烧处理,得到激光提纯石英块体;激光提纯石英块体经氢氟酸清洗表面以脱除方石英析晶层,得到3N级石英块体;3N级石英块体进行精细洁净制粉得到3N级石英粉,3N级石英粉加入到酸性溶液中酸浸深度除杂得到4N级以上再生高纯石英粉;4N级以上再生高纯石英粉经纯水清洗,烘干得到4N级以上再生高纯石英粉产品。
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