一种用于制备光学ZnS或ZnSe材料的CVD装置及方法

By designing a multifunctional CVD device, H2S/H2Se is introduced using Ar gas to react with Zn vapor on the mold surface, solving the problems of uniformity and singleness in the preparation of existing equipment. This enables the batch preparation of high-quality ZnS and ZnSe materials and simplifies the subsequent processing procedures.

CN117802478BActive Publication Date: 2026-07-17KUNMING KAIHANG PHOTOELECTRIC TECH CO LTD

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
KUNMING KAIHANG PHOTOELECTRIC TECH CO LTD
Filing Date
2024-01-02
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Existing CVD equipment can only prepare ZnS materials, which has a narrow range of applications, makes it difficult to maintain the stoichiometry, and the large particle size of the prepared ZnS affects optical transmittance and uniformity. It is also impossible to prepare optical ZnS and ZnSe blanks of specific shapes, which increases the need for subsequent grinding and polishing processes.

Method used

Design a CVD device including a main frame, insulation structure, water circulation structure, heating structure and air intake structure. The zinc block is directly heated at the bottom of the vacuum furnace to vaporize it. Ar gas is used as a carrier gas to introduce H2S/H2Se for chemical reaction and deposited onto the mold surface to form a high-quality optical blank. The mold design enables the batch preparation of different shapes.

Benefits of technology

The method enables diversified preparation of ZnS and ZnSe materials, improves material uniformity and optical quality, reduces the difficulty of subsequent processing, and enhances preparation efficiency and flexibility. The transmittance of the prepared materials is significantly improved.

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Abstract

本发明涉及一种用于制备光学ZnS或ZnSe材料的CVD装置及方法;包括主体框架,所述主体框架由上炉体与下炉体组成;所述上炉体与下炉体通过设置在上炉体与下炉体外壁上的连接合叶和锁扣连接;实现上炉体与下炉体的开关和密闭;主体框架内部设置CVD空腔;所述CVD装置包括以下功能机构:保温结构、水循环结构、加热结构、进气结构。本发明通过在真空炉底部直接加热锌块使其气化,用氩气作为载气将H2S送入反应器,将三种气态原材料导入到一个沉积坩埚模具内,使其发生化学反应,形成硫化锌或硒化锌,并沉积到模具表面上,沉积模具既是反应腔室也是光学坯料沉积模具,最终形成高质量的光学坯料。
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