一种采用集成膜甲醇分离器系统制备高纯度甲醇的方法

By integrating a membrane methanol separator system and combining multi-stage separation technology with modified filter membranes, the problems of complex and energy-intensive preparation of high-purity methanol in existing technologies have been solved, achieving efficient and low-cost preparation of high-purity methanol and effective removal of trimethylamine content.

CN117899553BActive Publication Date: 2026-07-17ZHEJIANG HONGSHI ENVIRONMENTAL PROTECTION SCI & TECH

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
ZHEJIANG HONGSHI ENVIRONMENTAL PROTECTION SCI & TECH
Filing Date
2023-12-21
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Existing technologies for preparing high-purity methanol suffer from problems such as complex preparation processes, high energy consumption, low economic efficiency, and difficulty in effectively removing impurities from light and heavy fractions. In particular, the trimethylamine content is difficult to meet the requirements of propylene production processes.

Method used

An integrated membrane methanol separator system is adopted, which combines mechanical cyclone separation, membrane separation and atomization absorption technology. Modified polyethersulfone microporous filter membrane and stainless steel metal fiber sintered material are used to adsorb polar impurities through multi-stage high-precision separation and electrostatic induction, thereby improving the purity of methanol.

Benefits of technology

It has achieved efficient and low-cost preparation of high-purity methanol with a purity of 99.99% and a trimethylamine content of less than 2x10-9, meeting the requirements of propylene production process, while reducing equipment investment and energy consumption.

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Abstract

本发明涉及甲醇生成技术领域,具体关于一种采用集成膜甲醇分离器系统制备高纯度甲醇的方法;本发明提出了一种采用集成膜甲醇分离器系统,将粗甲醇提纯得到高纯度甲醇的方法;集成膜甲醇分离器系统包括一级机械式旋流分离装置,二级膜分离装置,一级雾化吸收分离装置;集成膜甲醇分离技术是将机械式旋流分离技术、膜分离技术、吸收分离技术有机组合,采用经济、合理的结构设计,使工艺中的甲醇(含其它液、固杂质)在低速、多级、高精度条件下得到高效分离的一项复合技术;本发明通过高效吸收及多级高精度的分离,集成膜甲醇分离器制得的甲醇含量可达到99.99%以上,同时出口气体甲醇含量可控制在0.1%以下。
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