一轴四径式准全径向流氨合成反应器的氨合成方法

By designing a quasi-radial flow ammonia synthesis reactor with a single axis and four diameters, and employing a parallel flow of split reaction gases and a snap ring-type self-sealing internal component, the temperature and gas distribution of the catalyst bed were optimized, the problem of limited synthesis tower diameter was solved, and a highly efficient ammonia synthesis reaction was achieved, improving the net ammonia value and reaction efficiency.

CN117920063BActive Publication Date: 2026-07-17NANJING JUTUO CHEM TECH

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
NANJING JUTUO CHEM TECH
Filing Date
2024-01-24
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

How can we optimize the design of a multi-bed reactor with a relatively small diameter, a large height-to-diameter ratio, a large catalyst loading, and a high ammonia net value under the condition of limited synthesis tower diameter, so as to improve the efficiency of ammonia synthesis reaction?

Method used

A quasi-radial flow ammonia synthesis reactor with a single axis and four diameters is adopted. The reactant gas enters the catalyst bed in parallel through a split flow. The internal components are designed with a snap ring type self-sealing. Combined with a high-efficiency heat exchanger and baffle elements, the temperature and gas distribution of the catalyst bed are optimized to achieve high-efficiency multi-bed reaction.

Benefits of technology

It increases the net ammonia content at the reactor outlet to over 21%, which is nearly 3% higher than that of a traditional three-bed, three-stage reactor. Furthermore, the catalyst bed can be maintained independently, saving on equipment investment. It is suitable for reaction gases with low inlet ammonia content.

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Abstract

本申请公开了一轴四径准全径向流氨合成反应器的氨合成方法,反应器具有外壳和内件,内件内自上而下依次设置有轴向催化剂床层、第一、第二、第三和第四径向催化剂床层,第一、第二、第三径向催化剂床层内分别设有上、中、下部换热器,第四径向催化剂床层内设有反应气集气管;轴向催化剂床层内设有气体分布器,轴向催化剂床层和第一径向催化剂床层内设有中部冷激管;第一、三、四、五股反应气被加热后进入轴向催化剂床层进行反应,再依次进入第二、三、四径向催化剂床层反应,反应后气体经反应气集气管流出反应器。通过采用各换热器分流气加热后以“并联”方式进入“零米”的气体工艺布置方式,可以使得反应器出口氨净值高达21%以上。
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