一种用于油气回收的成型颗粒炭的制备方法

By forming a three-dimensional cross-linked gel structure with chitosan, terminal amino polyether, and octa(aminophenyltrioxosilane), the problems of cumbersome preparation process and low strength in the existing particulate carbon technology are solved. This enables the preparation of molded particulate carbon with high strength and high adsorption performance, simplifies the process, and improves the working capacity of butane.

CN118002081BActive Publication Date: 2026-07-17FUJIAN XINSEN CARBON
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
FUJIAN XINSEN CARBON
Filing Date
2024-03-07
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Existing technologies for preparing granular activated carbon involve cumbersome processes and the use of inorganic binders that cause pore blockage, reducing butane working capacity and making it difficult to simultaneously achieve high strength and high adsorption performance.

Method used

Chitosan and terminal amino polyethers were used as organic binders to form a three-dimensional cross-linked gel structure with octa(aminophenyltrioxosilane). Molded granular carbon was prepared by freeze drying, avoiding the high-temperature carbonization step. The cross-linking reaction was further carried out using an aliphatic dialdehyde solution for shaping.

Benefits of technology

High-strength shaped granular carbon with high butane working capacity was prepared, simplifying the process steps and saving energy and being environmentally friendly.

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Abstract

一种用于油气回收的成型颗粒炭的制备方法,包括如下步骤:1)将壳聚糖、端胺基聚醚加入水中,加酸并搅拌至无不溶物的混合溶液,加入八(氨基苯基三氧硅烷)超声分散,得悬浮液备用;2)向步骤1)悬浮液中加入活性炭粉混合、捏合、造粒、干燥,得前驱体;3)将步骤2)所得前驱体浸泡于脂肪族二元醛溶液进行反应,反应结束后过滤、静置老化、洗涤、预冻、冷冻干燥即得上述用于油气回收的成型颗粒炭,所得颗粒炭不仅强度高,同时兼具较高的丁烷工作容量值。
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